2-Hy­droxy-N′-(4-hy­droxy­benzyl­idene)-3-methyl­benzohydrazide

The title compound, C(15)H(14)N(2)O(3), was prepared by condensing 4-hy­droxy­benzaldehyde and 2-hy­droxy-3-methyl­benzo­hydra­zide in methanol. The two benzene rings make a dihedral angle of 19.03 (11)°. An intra­molecular O—H⋯O hydrogen bond is observed. The crystal structure is stabilized by inte...

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Detalles Bibliográficos
Autores principales: Shen, Xi-Hai, Zhu, Li-Xue, Shao, Li-Juen, Zhu, Zhao-Fu
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3274990/
https://www.ncbi.nlm.nih.gov/pubmed/22346935
http://dx.doi.org/10.1107/S1600536811055930
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author Shen, Xi-Hai
Zhu, Li-Xue
Shao, Li-Juen
Zhu, Zhao-Fu
author_facet Shen, Xi-Hai
Zhu, Li-Xue
Shao, Li-Juen
Zhu, Zhao-Fu
author_sort Shen, Xi-Hai
collection PubMed
description The title compound, C(15)H(14)N(2)O(3), was prepared by condensing 4-hy­droxy­benzaldehyde and 2-hy­droxy-3-methyl­benzo­hydra­zide in methanol. The two benzene rings make a dihedral angle of 19.03 (11)°. An intra­molecular O—H⋯O hydrogen bond is observed. The crystal structure is stabilized by inter­molecular O—H⋯O and N—H⋯O hydrogen bonds and C—H⋯O inter­actions, which lead to the formation of a three-dimensional network.
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spelling pubmed-32749902012-02-15 2-Hy­droxy-N′-(4-hy­droxy­benzyl­idene)-3-methyl­benzohydrazide Shen, Xi-Hai Zhu, Li-Xue Shao, Li-Juen Zhu, Zhao-Fu Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(15)H(14)N(2)O(3), was prepared by condensing 4-hy­droxy­benzaldehyde and 2-hy­droxy-3-methyl­benzo­hydra­zide in methanol. The two benzene rings make a dihedral angle of 19.03 (11)°. An intra­molecular O—H⋯O hydrogen bond is observed. The crystal structure is stabilized by inter­molecular O—H⋯O and N—H⋯O hydrogen bonds and C—H⋯O inter­actions, which lead to the formation of a three-dimensional network. International Union of Crystallography 2012-01-07 /pmc/articles/PMC3274990/ /pubmed/22346935 http://dx.doi.org/10.1107/S1600536811055930 Text en © Shen et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Shen, Xi-Hai
Zhu, Li-Xue
Shao, Li-Juen
Zhu, Zhao-Fu
2-Hy­droxy-N′-(4-hy­droxy­benzyl­idene)-3-methyl­benzohydrazide
title 2-Hy­droxy-N′-(4-hy­droxy­benzyl­idene)-3-methyl­benzohydrazide
title_full 2-Hy­droxy-N′-(4-hy­droxy­benzyl­idene)-3-methyl­benzohydrazide
title_fullStr 2-Hy­droxy-N′-(4-hy­droxy­benzyl­idene)-3-methyl­benzohydrazide
title_full_unstemmed 2-Hy­droxy-N′-(4-hy­droxy­benzyl­idene)-3-methyl­benzohydrazide
title_short 2-Hy­droxy-N′-(4-hy­droxy­benzyl­idene)-3-methyl­benzohydrazide
title_sort 2-hy­droxy-n′-(4-hy­droxy­benzyl­idene)-3-methyl­benzohydrazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3274990/
https://www.ncbi.nlm.nih.gov/pubmed/22346935
http://dx.doi.org/10.1107/S1600536811055930
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AT shaolijuen 2hydroxyn4hydroxybenzylidene3methylbenzohydrazide
AT zhuzhaofu 2hydroxyn4hydroxybenzylidene3methylbenzohydrazide

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