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(3S,4Z)-3-Chloro-1-methyl-4-[(2E)-(3-methylbenzylidene)hydrazinylidene]-3,4-dihydro-1H-2,1-benzothiazine 2,2-dioxide
In the title compound, C(17)H(16)ClN(3)O(2)S, the dihedral angle between the benzene rings is 7.75 (13)°. The thiazine ring adopts an envelope conformation with the S atom as the flap at a distance of 0.813 (2) Å from the plane through the other five atoms. In the crystal, C—H⋯O hydrogen bonds link...
Autores principales: | , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2012
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3275023/ https://www.ncbi.nlm.nih.gov/pubmed/22346968 http://dx.doi.org/10.1107/S1600536811056315 |
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author | Shafiq, Muhammad Tahir, M. Nawaz Khan, Islam Ullah Zia-Ur-Rehman, Muhammad |
author_facet | Shafiq, Muhammad Tahir, M. Nawaz Khan, Islam Ullah Zia-Ur-Rehman, Muhammad |
author_sort | Shafiq, Muhammad |
collection | PubMed |
description | In the title compound, C(17)H(16)ClN(3)O(2)S, the dihedral angle between the benzene rings is 7.75 (13)°. The thiazine ring adopts an envelope conformation with the S atom as the flap at a distance of 0.813 (2) Å from the plane through the other five atoms. In the crystal, C—H⋯O hydrogen bonds link the molecules into chains propagating in [100]. |
format | Online Article Text |
id | pubmed-3275023 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2012 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-32750232012-02-15 (3S,4Z)-3-Chloro-1-methyl-4-[(2E)-(3-methylbenzylidene)hydrazinylidene]-3,4-dihydro-1H-2,1-benzothiazine 2,2-dioxide Shafiq, Muhammad Tahir, M. Nawaz Khan, Islam Ullah Zia-Ur-Rehman, Muhammad Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(17)H(16)ClN(3)O(2)S, the dihedral angle between the benzene rings is 7.75 (13)°. The thiazine ring adopts an envelope conformation with the S atom as the flap at a distance of 0.813 (2) Å from the plane through the other five atoms. In the crystal, C—H⋯O hydrogen bonds link the molecules into chains propagating in [100]. International Union of Crystallography 2012-01-11 /pmc/articles/PMC3275023/ /pubmed/22346968 http://dx.doi.org/10.1107/S1600536811056315 Text en © Shafiq et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Shafiq, Muhammad Tahir, M. Nawaz Khan, Islam Ullah Zia-Ur-Rehman, Muhammad (3S,4Z)-3-Chloro-1-methyl-4-[(2E)-(3-methylbenzylidene)hydrazinylidene]-3,4-dihydro-1H-2,1-benzothiazine 2,2-dioxide |
title | (3S,4Z)-3-Chloro-1-methyl-4-[(2E)-(3-methylbenzylidene)hydrazinylidene]-3,4-dihydro-1H-2,1-benzothiazine 2,2-dioxide |
title_full | (3S,4Z)-3-Chloro-1-methyl-4-[(2E)-(3-methylbenzylidene)hydrazinylidene]-3,4-dihydro-1H-2,1-benzothiazine 2,2-dioxide |
title_fullStr | (3S,4Z)-3-Chloro-1-methyl-4-[(2E)-(3-methylbenzylidene)hydrazinylidene]-3,4-dihydro-1H-2,1-benzothiazine 2,2-dioxide |
title_full_unstemmed | (3S,4Z)-3-Chloro-1-methyl-4-[(2E)-(3-methylbenzylidene)hydrazinylidene]-3,4-dihydro-1H-2,1-benzothiazine 2,2-dioxide |
title_short | (3S,4Z)-3-Chloro-1-methyl-4-[(2E)-(3-methylbenzylidene)hydrazinylidene]-3,4-dihydro-1H-2,1-benzothiazine 2,2-dioxide |
title_sort | (3s,4z)-3-chloro-1-methyl-4-[(2e)-(3-methylbenzylidene)hydrazinylidene]-3,4-dihydro-1h-2,1-benzothiazine 2,2-dioxide |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3275023/ https://www.ncbi.nlm.nih.gov/pubmed/22346968 http://dx.doi.org/10.1107/S1600536811056315 |
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