(E)-1-(3-Eth­oxy-2-hy­droxy­benzyl­idene)thio­semicarbazide

The title compound, C(10)H(13)N(3)O(2)S, crystallizes with two independent mol­ecules (A and B) in the asymmetric unit. In the crystal, the A and B mol­ecules are linked via pairs of N—H⋯O and O—H⋯S hydrogen bonds, forming dimers with R (2) (2)(14) and R (2) (2)(6) ring motifs. These dimers are link...

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Detalles Bibliográficos
Autores principales: Adabi Ardakani, Amir, Kargar, Hadi, Kia, Reza, Tahir, Muhammad Nawaz
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3275025/
https://www.ncbi.nlm.nih.gov/pubmed/22346970
http://dx.doi.org/10.1107/S1600536812000487
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author Adabi Ardakani, Amir
Kargar, Hadi
Kia, Reza
Tahir, Muhammad Nawaz
author_facet Adabi Ardakani, Amir
Kargar, Hadi
Kia, Reza
Tahir, Muhammad Nawaz
author_sort Adabi Ardakani, Amir
collection PubMed
description The title compound, C(10)H(13)N(3)O(2)S, crystallizes with two independent mol­ecules (A and B) in the asymmetric unit. In the crystal, the A and B mol­ecules are linked via pairs of N—H⋯O and O—H⋯S hydrogen bonds, forming dimers with R (2) (2)(14) and R (2) (2)(6) ring motifs. These dimers are linked via a pair of N—H⋯S hydrogen bonds with an R (2) (2)(8) ring motif, forming chains propagating along the c-axis direction. The crystal was refined as an inversion twin with a final BASF ratio of 0.54 (11):0.46 (11).
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spelling pubmed-32750252012-02-15 (E)-1-(3-Eth­oxy-2-hy­droxy­benzyl­idene)thio­semicarbazide Adabi Ardakani, Amir Kargar, Hadi Kia, Reza Tahir, Muhammad Nawaz Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(10)H(13)N(3)O(2)S, crystallizes with two independent mol­ecules (A and B) in the asymmetric unit. In the crystal, the A and B mol­ecules are linked via pairs of N—H⋯O and O—H⋯S hydrogen bonds, forming dimers with R (2) (2)(14) and R (2) (2)(6) ring motifs. These dimers are linked via a pair of N—H⋯S hydrogen bonds with an R (2) (2)(8) ring motif, forming chains propagating along the c-axis direction. The crystal was refined as an inversion twin with a final BASF ratio of 0.54 (11):0.46 (11). International Union of Crystallography 2012-01-11 /pmc/articles/PMC3275025/ /pubmed/22346970 http://dx.doi.org/10.1107/S1600536812000487 Text en © Adabi Ardakani et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Adabi Ardakani, Amir
Kargar, Hadi
Kia, Reza
Tahir, Muhammad Nawaz
(E)-1-(3-Eth­oxy-2-hy­droxy­benzyl­idene)thio­semicarbazide
title (E)-1-(3-Eth­oxy-2-hy­droxy­benzyl­idene)thio­semicarbazide
title_full (E)-1-(3-Eth­oxy-2-hy­droxy­benzyl­idene)thio­semicarbazide
title_fullStr (E)-1-(3-Eth­oxy-2-hy­droxy­benzyl­idene)thio­semicarbazide
title_full_unstemmed (E)-1-(3-Eth­oxy-2-hy­droxy­benzyl­idene)thio­semicarbazide
title_short (E)-1-(3-Eth­oxy-2-hy­droxy­benzyl­idene)thio­semicarbazide
title_sort (e)-1-(3-eth­oxy-2-hy­droxy­benzyl­idene)thio­semicarbazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3275025/
https://www.ncbi.nlm.nih.gov/pubmed/22346970
http://dx.doi.org/10.1107/S1600536812000487
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AT kiareza e13ethoxy2hydroxybenzylidenethiosemicarbazide
AT tahirmuhammadnawaz e13ethoxy2hydroxybenzylidenethiosemicarbazide

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