Cargando…

N′-[(Z)-(1,5-Dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)methyl­idene]-2-hy­droxy­benzohydrazide

In the title compound, C(19)H(18)N(4)O(3), the pyrazole ring is oriented at dihedral angles of 41.12 (7) and 12.25 (10)°, respectively, with respect to the planes of the phenyl and benzene rings. Intra­molecular N—H⋯O and O—H⋯O hydrogen bonds generate seven- and six-membered S(7) and S(6) ring motif...

Descripción completa

Detalles Bibliográficos
Autores principales: Aslam, Muhammad, Anis, Itrat, Afza, Nighat, Ejaz, Khan, Islam Ullah, Arshad, Muhammad Nadeem
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3275035/
https://www.ncbi.nlm.nih.gov/pubmed/22346980
http://dx.doi.org/10.1107/S1600536812000402
_version_ 1782223160838455296
author Aslam, Muhammad
Anis, Itrat
Afza, Nighat
Ejaz,
Khan, Islam Ullah
Arshad, Muhammad Nadeem
author_facet Aslam, Muhammad
Anis, Itrat
Afza, Nighat
Ejaz,
Khan, Islam Ullah
Arshad, Muhammad Nadeem
author_sort Aslam, Muhammad
collection PubMed
description In the title compound, C(19)H(18)N(4)O(3), the pyrazole ring is oriented at dihedral angles of 41.12 (7) and 12.25 (10)°, respectively, with respect to the planes of the phenyl and benzene rings. Intra­molecular N—H⋯O and O—H⋯O hydrogen bonds generate seven- and six-membered S(7) and S(6) ring motifs, respectively.
format Online
Article
Text
id pubmed-3275035
institution National Center for Biotechnology Information
language English
publishDate 2012
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-32750352012-02-15 N′-[(Z)-(1,5-Dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)methyl­idene]-2-hy­droxy­benzohydrazide Aslam, Muhammad Anis, Itrat Afza, Nighat Ejaz, Khan, Islam Ullah Arshad, Muhammad Nadeem Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(19)H(18)N(4)O(3), the pyrazole ring is oriented at dihedral angles of 41.12 (7) and 12.25 (10)°, respectively, with respect to the planes of the phenyl and benzene rings. Intra­molecular N—H⋯O and O—H⋯O hydrogen bonds generate seven- and six-membered S(7) and S(6) ring motifs, respectively. International Union of Crystallography 2012-01-11 /pmc/articles/PMC3275035/ /pubmed/22346980 http://dx.doi.org/10.1107/S1600536812000402 Text en © Aslam et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Aslam, Muhammad
Anis, Itrat
Afza, Nighat
Ejaz,
Khan, Islam Ullah
Arshad, Muhammad Nadeem
N′-[(Z)-(1,5-Dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)methyl­idene]-2-hy­droxy­benzohydrazide
title N′-[(Z)-(1,5-Dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)methyl­idene]-2-hy­droxy­benzohydrazide
title_full N′-[(Z)-(1,5-Dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)methyl­idene]-2-hy­droxy­benzohydrazide
title_fullStr N′-[(Z)-(1,5-Dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)methyl­idene]-2-hy­droxy­benzohydrazide
title_full_unstemmed N′-[(Z)-(1,5-Dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)methyl­idene]-2-hy­droxy­benzohydrazide
title_short N′-[(Z)-(1,5-Dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)methyl­idene]-2-hy­droxy­benzohydrazide
title_sort n′-[(z)-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1h-pyrazol-4-yl)methyl­idene]-2-hy­droxy­benzohydrazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3275035/
https://www.ncbi.nlm.nih.gov/pubmed/22346980
http://dx.doi.org/10.1107/S1600536812000402
work_keys_str_mv AT aslammuhammad nz15dimethyl3oxo2phenyl23dihydro1hpyrazol4ylmethylidene2hydroxybenzohydrazide
AT anisitrat nz15dimethyl3oxo2phenyl23dihydro1hpyrazol4ylmethylidene2hydroxybenzohydrazide
AT afzanighat nz15dimethyl3oxo2phenyl23dihydro1hpyrazol4ylmethylidene2hydroxybenzohydrazide
AT ejaz nz15dimethyl3oxo2phenyl23dihydro1hpyrazol4ylmethylidene2hydroxybenzohydrazide
AT khanislamullah nz15dimethyl3oxo2phenyl23dihydro1hpyrazol4ylmethylidene2hydroxybenzohydrazide
AT arshadmuhammadnadeem nz15dimethyl3oxo2phenyl23dihydro1hpyrazol4ylmethylidene2hydroxybenzohydrazide