4-Hy­droxy-3,5-dimeth­oxy-N-{4-[(5-methyl-1,2-oxazol-3-yl)sulfamo­yl]phen­yl}benzamide methanol monosolvate

The title compound, C(19)H(19)N(3)O(7)S·CH(3)OH, was synthesized from syringic acid and sulfamethoxazole. The benzene rings make a dihedral angle of 41.8 (1)° and the isoxazole ring is twisted by 74.3 (1)° from the central benzene ring. The crystal packing features O—H⋯O and O—H⋯N hydrogen bonds in...

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Autores principales: Pan, Wei-Gao, Zhao, Zhi-Dong, Luo, Peng, Lin, Cui-Wu, Miao, Jian-Hua
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3275057/
https://www.ncbi.nlm.nih.gov/pubmed/22347002
http://dx.doi.org/10.1107/S1600536811055991
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author Pan, Wei-Gao
Zhao, Zhi-Dong
Luo, Peng
Lin, Cui-Wu
Miao, Jian-Hua
author_facet Pan, Wei-Gao
Zhao, Zhi-Dong
Luo, Peng
Lin, Cui-Wu
Miao, Jian-Hua
author_sort Pan, Wei-Gao
collection PubMed
description The title compound, C(19)H(19)N(3)O(7)S·CH(3)OH, was synthesized from syringic acid and sulfamethoxazole. The benzene rings make a dihedral angle of 41.8 (1)° and the isoxazole ring is twisted by 74.3 (1)° from the central benzene ring. The crystal packing features O—H⋯O and O—H⋯N hydrogen bonds in which the hy­droxy groups from the main mol­ecule and methanol solvent mol­ecules serve as donor groups.
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spelling pubmed-32750572012-02-15 4-Hy­droxy-3,5-dimeth­oxy-N-{4-[(5-methyl-1,2-oxazol-3-yl)sulfamo­yl]phen­yl}benzamide methanol monosolvate Pan, Wei-Gao Zhao, Zhi-Dong Luo, Peng Lin, Cui-Wu Miao, Jian-Hua Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(19)H(19)N(3)O(7)S·CH(3)OH, was synthesized from syringic acid and sulfamethoxazole. The benzene rings make a dihedral angle of 41.8 (1)° and the isoxazole ring is twisted by 74.3 (1)° from the central benzene ring. The crystal packing features O—H⋯O and O—H⋯N hydrogen bonds in which the hy­droxy groups from the main mol­ecule and methanol solvent mol­ecules serve as donor groups. International Union of Crystallography 2012-01-14 /pmc/articles/PMC3275057/ /pubmed/22347002 http://dx.doi.org/10.1107/S1600536811055991 Text en © Pan et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Pan, Wei-Gao
Zhao, Zhi-Dong
Luo, Peng
Lin, Cui-Wu
Miao, Jian-Hua
4-Hy­droxy-3,5-dimeth­oxy-N-{4-[(5-methyl-1,2-oxazol-3-yl)sulfamo­yl]phen­yl}benzamide methanol monosolvate
title 4-Hy­droxy-3,5-dimeth­oxy-N-{4-[(5-methyl-1,2-oxazol-3-yl)sulfamo­yl]phen­yl}benzamide methanol monosolvate
title_full 4-Hy­droxy-3,5-dimeth­oxy-N-{4-[(5-methyl-1,2-oxazol-3-yl)sulfamo­yl]phen­yl}benzamide methanol monosolvate
title_fullStr 4-Hy­droxy-3,5-dimeth­oxy-N-{4-[(5-methyl-1,2-oxazol-3-yl)sulfamo­yl]phen­yl}benzamide methanol monosolvate
title_full_unstemmed 4-Hy­droxy-3,5-dimeth­oxy-N-{4-[(5-methyl-1,2-oxazol-3-yl)sulfamo­yl]phen­yl}benzamide methanol monosolvate
title_short 4-Hy­droxy-3,5-dimeth­oxy-N-{4-[(5-methyl-1,2-oxazol-3-yl)sulfamo­yl]phen­yl}benzamide methanol monosolvate
title_sort 4-hy­droxy-3,5-dimeth­oxy-n-{4-[(5-methyl-1,2-oxazol-3-yl)sulfamo­yl]phen­yl}benzamide methanol monosolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3275057/
https://www.ncbi.nlm.nih.gov/pubmed/22347002
http://dx.doi.org/10.1107/S1600536811055991
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