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2-[(E)-4-Diethyl­amino-2-hy­droxy­benzyl­idene]hydrazinecarboxamide

Two mol­ecules make up the asymmetric unit of the title compound, C(12)H(18)N(4)O(2), and both feature an intra­molecular O—H⋯N hydrogen bond, which generates an S(6) ring. The diethyl­amino group of one of the mol­ecules is disordered over two sets of sites in a 0.59 (2):0.41 (2) ratio. In the crys...

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Autores principales: Fun, Hoong-Kun, Ooi, Chin Wei, Malladi, Shridhar, Isloor, Arun M., Shivananda, Kammasandra N.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3275058/
https://www.ncbi.nlm.nih.gov/pubmed/22347003
http://dx.doi.org/10.1107/S1600536812000311
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author Fun, Hoong-Kun
Ooi, Chin Wei
Malladi, Shridhar
Isloor, Arun M.
Shivananda, Kammasandra N.
author_facet Fun, Hoong-Kun
Ooi, Chin Wei
Malladi, Shridhar
Isloor, Arun M.
Shivananda, Kammasandra N.
author_sort Fun, Hoong-Kun
collection PubMed
description Two mol­ecules make up the asymmetric unit of the title compound, C(12)H(18)N(4)O(2), and both feature an intra­molecular O—H⋯N hydrogen bond, which generates an S(6) ring. The diethyl­amino group of one of the mol­ecules is disordered over two sets of sites in a 0.59 (2):0.41 (2) ratio. In the crystal, N—H⋯O hydrogen bonds link the mol­ecules into sheets lying parallel to the ac plane and C—H⋯π inter­actions are also observed.
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spelling pubmed-32750582012-02-15 2-[(E)-4-Diethyl­amino-2-hy­droxy­benzyl­idene]hydrazinecarboxamide Fun, Hoong-Kun Ooi, Chin Wei Malladi, Shridhar Isloor, Arun M. Shivananda, Kammasandra N. Acta Crystallogr Sect E Struct Rep Online Organic Papers Two mol­ecules make up the asymmetric unit of the title compound, C(12)H(18)N(4)O(2), and both feature an intra­molecular O—H⋯N hydrogen bond, which generates an S(6) ring. The diethyl­amino group of one of the mol­ecules is disordered over two sets of sites in a 0.59 (2):0.41 (2) ratio. In the crystal, N—H⋯O hydrogen bonds link the mol­ecules into sheets lying parallel to the ac plane and C—H⋯π inter­actions are also observed. International Union of Crystallography 2012-01-14 /pmc/articles/PMC3275058/ /pubmed/22347003 http://dx.doi.org/10.1107/S1600536812000311 Text en © Fun et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Fun, Hoong-Kun
Ooi, Chin Wei
Malladi, Shridhar
Isloor, Arun M.
Shivananda, Kammasandra N.
2-[(E)-4-Diethyl­amino-2-hy­droxy­benzyl­idene]hydrazinecarboxamide
title 2-[(E)-4-Diethyl­amino-2-hy­droxy­benzyl­idene]hydrazinecarboxamide
title_full 2-[(E)-4-Diethyl­amino-2-hy­droxy­benzyl­idene]hydrazinecarboxamide
title_fullStr 2-[(E)-4-Diethyl­amino-2-hy­droxy­benzyl­idene]hydrazinecarboxamide
title_full_unstemmed 2-[(E)-4-Diethyl­amino-2-hy­droxy­benzyl­idene]hydrazinecarboxamide
title_short 2-[(E)-4-Diethyl­amino-2-hy­droxy­benzyl­idene]hydrazinecarboxamide
title_sort 2-[(e)-4-diethyl­amino-2-hy­droxy­benzyl­idene]hydrazinecarboxamide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3275058/
https://www.ncbi.nlm.nih.gov/pubmed/22347003
http://dx.doi.org/10.1107/S1600536812000311
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