(1R,2R,E,E)-N,N′-Bis(4-chloro­benzyl­idene)cyclo­hexane-1,2-diamine

The title Schiff base ligand, C(20)H(20)Cl(2)N(2), was prepared by condensation of commercially available p-chloro­benzalde­hyde and (R,R)-1,2-diammonium­cyclo­hexane mono-(+)-tartrate. The cyclo­hexane ring adopts a chair conformation. The dihedral angle between the two aromatic rings is 62.52 (8)°...

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Detalles Bibliográficos
Autores principales: Arvinnezhad, Hamid, Jadidi, Khosrow, Notash, Behrouz
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3275080/
https://www.ncbi.nlm.nih.gov/pubmed/22347025
http://dx.doi.org/10.1107/S1600536812000724
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author Arvinnezhad, Hamid
Jadidi, Khosrow
Notash, Behrouz
author_facet Arvinnezhad, Hamid
Jadidi, Khosrow
Notash, Behrouz
author_sort Arvinnezhad, Hamid
collection PubMed
description The title Schiff base ligand, C(20)H(20)Cl(2)N(2), was prepared by condensation of commercially available p-chloro­benzalde­hyde and (R,R)-1,2-diammonium­cyclo­hexane mono-(+)-tartrate. The cyclo­hexane ring adopts a chair conformation. The dihedral angle between the two aromatic rings is 62.52 (8)°. The crystal structure is stabilized by an inter­molecular C—H⋯Cl hydrogen bond.
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spelling pubmed-32750802012-02-15 (1R,2R,E,E)-N,N′-Bis(4-chloro­benzyl­idene)cyclo­hexane-1,2-diamine Arvinnezhad, Hamid Jadidi, Khosrow Notash, Behrouz Acta Crystallogr Sect E Struct Rep Online Organic Papers The title Schiff base ligand, C(20)H(20)Cl(2)N(2), was prepared by condensation of commercially available p-chloro­benzalde­hyde and (R,R)-1,2-diammonium­cyclo­hexane mono-(+)-tartrate. The cyclo­hexane ring adopts a chair conformation. The dihedral angle between the two aromatic rings is 62.52 (8)°. The crystal structure is stabilized by an inter­molecular C—H⋯Cl hydrogen bond. International Union of Crystallography 2012-01-14 /pmc/articles/PMC3275080/ /pubmed/22347025 http://dx.doi.org/10.1107/S1600536812000724 Text en © Arvinnezhad et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Arvinnezhad, Hamid
Jadidi, Khosrow
Notash, Behrouz
(1R,2R,E,E)-N,N′-Bis(4-chloro­benzyl­idene)cyclo­hexane-1,2-diamine
title (1R,2R,E,E)-N,N′-Bis(4-chloro­benzyl­idene)cyclo­hexane-1,2-diamine
title_full (1R,2R,E,E)-N,N′-Bis(4-chloro­benzyl­idene)cyclo­hexane-1,2-diamine
title_fullStr (1R,2R,E,E)-N,N′-Bis(4-chloro­benzyl­idene)cyclo­hexane-1,2-diamine
title_full_unstemmed (1R,2R,E,E)-N,N′-Bis(4-chloro­benzyl­idene)cyclo­hexane-1,2-diamine
title_short (1R,2R,E,E)-N,N′-Bis(4-chloro­benzyl­idene)cyclo­hexane-1,2-diamine
title_sort (1r,2r,e,e)-n,n′-bis(4-chloro­benzyl­idene)cyclo­hexane-1,2-diamine
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3275080/
https://www.ncbi.nlm.nih.gov/pubmed/22347025
http://dx.doi.org/10.1107/S1600536812000724
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AT notashbehrouz 1r2reennbis4chlorobenzylidenecyclohexane12diamine

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