N,N-Diethyl-2-hy­droxy­ethanaminium 5-(5-chloro-2,4-dinitro­phen­yl)-2,6-dioxo-1,2,3,6-tetra­hydro­pyrimidin-4-olate hemihydrate

The asymmetric unit of the title salt, C(6)H(16)NO(+)·C(10)H(4)ClN(4)O(7) (−)·0.5H(2)O, contains two cations, two anions and one water mol­ecule. In one independent anion, one nitro group is rotationally disordered over two orientations in a 0.657 (8):0.343 (8) ratio. In the crystal, inter­molecular...

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Detalles Bibliográficos
Autores principales: Babykala, Rajamanickam, Kalaivani, Doraisamyraja
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3275279/
https://www.ncbi.nlm.nih.gov/pubmed/22347135
http://dx.doi.org/10.1107/S1600536812003248
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author Babykala, Rajamanickam
Kalaivani, Doraisamyraja
author_facet Babykala, Rajamanickam
Kalaivani, Doraisamyraja
author_sort Babykala, Rajamanickam
collection PubMed
description The asymmetric unit of the title salt, C(6)H(16)NO(+)·C(10)H(4)ClN(4)O(7) (−)·0.5H(2)O, contains two cations, two anions and one water mol­ecule. In one independent anion, one nitro group is rotationally disordered over two orientations in a 0.657 (8):0.343 (8) ratio. In the crystal, inter­molecular N—H⋯O and O—H⋯O hydrogen bonds link all the components into ribbons extending along [100].
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spelling pubmed-32752792012-02-15 N,N-Diethyl-2-hy­droxy­ethanaminium 5-(5-chloro-2,4-dinitro­phen­yl)-2,6-dioxo-1,2,3,6-tetra­hydro­pyrimidin-4-olate hemihydrate Babykala, Rajamanickam Kalaivani, Doraisamyraja Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title salt, C(6)H(16)NO(+)·C(10)H(4)ClN(4)O(7) (−)·0.5H(2)O, contains two cations, two anions and one water mol­ecule. In one independent anion, one nitro group is rotationally disordered over two orientations in a 0.657 (8):0.343 (8) ratio. In the crystal, inter­molecular N—H⋯O and O—H⋯O hydrogen bonds link all the components into ribbons extending along [100]. International Union of Crystallography 2012-01-31 /pmc/articles/PMC3275279/ /pubmed/22347135 http://dx.doi.org/10.1107/S1600536812003248 Text en © Babykala and Kalaivani 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Babykala, Rajamanickam
Kalaivani, Doraisamyraja
N,N-Diethyl-2-hy­droxy­ethanaminium 5-(5-chloro-2,4-dinitro­phen­yl)-2,6-dioxo-1,2,3,6-tetra­hydro­pyrimidin-4-olate hemihydrate
title N,N-Diethyl-2-hy­droxy­ethanaminium 5-(5-chloro-2,4-dinitro­phen­yl)-2,6-dioxo-1,2,3,6-tetra­hydro­pyrimidin-4-olate hemihydrate
title_full N,N-Diethyl-2-hy­droxy­ethanaminium 5-(5-chloro-2,4-dinitro­phen­yl)-2,6-dioxo-1,2,3,6-tetra­hydro­pyrimidin-4-olate hemihydrate
title_fullStr N,N-Diethyl-2-hy­droxy­ethanaminium 5-(5-chloro-2,4-dinitro­phen­yl)-2,6-dioxo-1,2,3,6-tetra­hydro­pyrimidin-4-olate hemihydrate
title_full_unstemmed N,N-Diethyl-2-hy­droxy­ethanaminium 5-(5-chloro-2,4-dinitro­phen­yl)-2,6-dioxo-1,2,3,6-tetra­hydro­pyrimidin-4-olate hemihydrate
title_short N,N-Diethyl-2-hy­droxy­ethanaminium 5-(5-chloro-2,4-dinitro­phen­yl)-2,6-dioxo-1,2,3,6-tetra­hydro­pyrimidin-4-olate hemihydrate
title_sort n,n-diethyl-2-hy­droxy­ethanaminium 5-(5-chloro-2,4-dinitro­phen­yl)-2,6-dioxo-1,2,3,6-tetra­hydro­pyrimidin-4-olate hemihydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3275279/
https://www.ncbi.nlm.nih.gov/pubmed/22347135
http://dx.doi.org/10.1107/S1600536812003248
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AT kalaivanidoraisamyraja nndiethyl2hydroxyethanaminium55chloro24dinitrophenyl26dioxo1236tetrahydropyrimidin4olatehemihydrate

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