(E)-4-Hy­droxy-N′-(2-hy­droxy-3,5-diiodo­benzyl­idene)-3-meth­oxy­benzohydrazide methanol monosolvate

In the title compound, C(15)H(12)I(2)N(2)O(4)·CH(3)OH, the hydrazone mol­ecule exists in an E conformation with respect to the C=N bond. The dihedral angle between the rings is 11.9 (2)°. There is one intra­molecular O—H⋯N hydrogen bond in the hydrazone mol­ecule. In the crystal, the hydrazone and m...

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Autor principal: Li, Xiao-Yan
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3295446/
https://www.ncbi.nlm.nih.gov/pubmed/22412557
http://dx.doi.org/10.1107/S1600536812004552
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author Li, Xiao-Yan
author_facet Li, Xiao-Yan
author_sort Li, Xiao-Yan
collection PubMed
description In the title compound, C(15)H(12)I(2)N(2)O(4)·CH(3)OH, the hydrazone mol­ecule exists in an E conformation with respect to the C=N bond. The dihedral angle between the rings is 11.9 (2)°. There is one intra­molecular O—H⋯N hydrogen bond in the hydrazone mol­ecule. In the crystal, the hydrazone and methanol mol­ecules are linked through O—H⋯O and N—H⋯O hydrogen bonds and C—H⋯O inter­actions to form two-dimensional networks lying parallel to (001).
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spelling pubmed-32954462012-03-12 (E)-4-Hy­droxy-N′-(2-hy­droxy-3,5-diiodo­benzyl­idene)-3-meth­oxy­benzohydrazide methanol monosolvate Li, Xiao-Yan Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(15)H(12)I(2)N(2)O(4)·CH(3)OH, the hydrazone mol­ecule exists in an E conformation with respect to the C=N bond. The dihedral angle between the rings is 11.9 (2)°. There is one intra­molecular O—H⋯N hydrogen bond in the hydrazone mol­ecule. In the crystal, the hydrazone and methanol mol­ecules are linked through O—H⋯O and N—H⋯O hydrogen bonds and C—H⋯O inter­actions to form two-dimensional networks lying parallel to (001). International Union of Crystallography 2012-02-10 /pmc/articles/PMC3295446/ /pubmed/22412557 http://dx.doi.org/10.1107/S1600536812004552 Text en © Xiao-Yan Li 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Li, Xiao-Yan
(E)-4-Hy­droxy-N′-(2-hy­droxy-3,5-diiodo­benzyl­idene)-3-meth­oxy­benzohydrazide methanol monosolvate
title (E)-4-Hy­droxy-N′-(2-hy­droxy-3,5-diiodo­benzyl­idene)-3-meth­oxy­benzohydrazide methanol monosolvate
title_full (E)-4-Hy­droxy-N′-(2-hy­droxy-3,5-diiodo­benzyl­idene)-3-meth­oxy­benzohydrazide methanol monosolvate
title_fullStr (E)-4-Hy­droxy-N′-(2-hy­droxy-3,5-diiodo­benzyl­idene)-3-meth­oxy­benzohydrazide methanol monosolvate
title_full_unstemmed (E)-4-Hy­droxy-N′-(2-hy­droxy-3,5-diiodo­benzyl­idene)-3-meth­oxy­benzohydrazide methanol monosolvate
title_short (E)-4-Hy­droxy-N′-(2-hy­droxy-3,5-diiodo­benzyl­idene)-3-meth­oxy­benzohydrazide methanol monosolvate
title_sort (e)-4-hy­droxy-n′-(2-hy­droxy-3,5-diiodo­benzyl­idene)-3-meth­oxy­benzohydrazide methanol monosolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3295446/
https://www.ncbi.nlm.nih.gov/pubmed/22412557
http://dx.doi.org/10.1107/S1600536812004552
work_keys_str_mv AT lixiaoyan e4hydroxyn2hydroxy35diiodobenzylidene3methoxybenzohydrazidemethanolmonosolvate

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