N′-(2-Hy­droxy-4-meth­oxy­benzyl­idene)-4-methyl­benzohydrazide

The asymmetric unit of the title compound, C(16)H(16)N(2)O(3), contains four independent mol­ecules with different conformations; the dihedral angles between the two benzene rings in the mol­ecules are 39.7 (3), 45.4 (3), 50.6 (3) and 51.6 (3)°. Intramolecular O—H⋯N hydrogen bonds are observed in th...

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Detalles Bibliográficos
Autores principales: Zhang, Yan, Liu, Min, Ma, Jing-Jun
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3295464/
https://www.ncbi.nlm.nih.gov/pubmed/22412575
http://dx.doi.org/10.1107/S1600536812005156
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author Zhang, Yan
Liu, Min
Ma, Jing-Jun
author_facet Zhang, Yan
Liu, Min
Ma, Jing-Jun
author_sort Zhang, Yan
collection PubMed
description The asymmetric unit of the title compound, C(16)H(16)N(2)O(3), contains four independent mol­ecules with different conformations; the dihedral angles between the two benzene rings in the mol­ecules are 39.7 (3), 45.4 (3), 50.6 (3) and 51.6 (3)°. Intramolecular O—H⋯N hydrogen bonds are observed in the molecule. In the crystal, N—H⋯O hydrogen bonds link the mol­ecules into two crystallographically independent chains propagating in [010], and each chain is formed by two alternating independent mol­ecules. Weak C—H⋯O inter­actions also occur.
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spelling pubmed-32954642012-03-12 N′-(2-Hy­droxy-4-meth­oxy­benzyl­idene)-4-methyl­benzohydrazide Zhang, Yan Liu, Min Ma, Jing-Jun Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(16)H(16)N(2)O(3), contains four independent mol­ecules with different conformations; the dihedral angles between the two benzene rings in the mol­ecules are 39.7 (3), 45.4 (3), 50.6 (3) and 51.6 (3)°. Intramolecular O—H⋯N hydrogen bonds are observed in the molecule. In the crystal, N—H⋯O hydrogen bonds link the mol­ecules into two crystallographically independent chains propagating in [010], and each chain is formed by two alternating independent mol­ecules. Weak C—H⋯O inter­actions also occur. International Union of Crystallography 2012-02-10 /pmc/articles/PMC3295464/ /pubmed/22412575 http://dx.doi.org/10.1107/S1600536812005156 Text en © Zhang et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zhang, Yan
Liu, Min
Ma, Jing-Jun
N′-(2-Hy­droxy-4-meth­oxy­benzyl­idene)-4-methyl­benzohydrazide
title N′-(2-Hy­droxy-4-meth­oxy­benzyl­idene)-4-methyl­benzohydrazide
title_full N′-(2-Hy­droxy-4-meth­oxy­benzyl­idene)-4-methyl­benzohydrazide
title_fullStr N′-(2-Hy­droxy-4-meth­oxy­benzyl­idene)-4-methyl­benzohydrazide
title_full_unstemmed N′-(2-Hy­droxy-4-meth­oxy­benzyl­idene)-4-methyl­benzohydrazide
title_short N′-(2-Hy­droxy-4-meth­oxy­benzyl­idene)-4-methyl­benzohydrazide
title_sort n′-(2-hy­droxy-4-meth­oxy­benzyl­idene)-4-methyl­benzohydrazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3295464/
https://www.ncbi.nlm.nih.gov/pubmed/22412575
http://dx.doi.org/10.1107/S1600536812005156
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AT majingjun n2hydroxy4methoxybenzylidene4methylbenzohydrazide

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