3-Benzyl-6-methyl-2-sulfanylidene-2,3-di­hydroquinazolin-4(1H)-one

In the title compound, C(16)H(14)N(2)OS, the quinazoline ring system is essentially planar, with a maximum deviation of 0.029 (3) Å. The dihedral angle between the quinazoline and benzene rings is 88.4 (2)°. In the crystal, adjacent mol­ecules are connected via pairs of N—H⋯S and C—H⋯O hydrogen bond...

Descripción completa

Detalles Bibliográficos
Autores principales: Al-Salahi, Rashad, Al-Omar, Mohamed, El-Subbagh, Hussein, Hemamalini, Madhukar, Fun, Hoong-Kun
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3295489/
https://www.ncbi.nlm.nih.gov/pubmed/22412600
http://dx.doi.org/10.1107/S1600536812006009
_version_ 1782225589479931904
author Al-Salahi, Rashad
Al-Omar, Mohamed
El-Subbagh, Hussein
Hemamalini, Madhukar
Fun, Hoong-Kun
author_facet Al-Salahi, Rashad
Al-Omar, Mohamed
El-Subbagh, Hussein
Hemamalini, Madhukar
Fun, Hoong-Kun
author_sort Al-Salahi, Rashad
collection PubMed
description In the title compound, C(16)H(14)N(2)OS, the quinazoline ring system is essentially planar, with a maximum deviation of 0.029 (3) Å. The dihedral angle between the quinazoline and benzene rings is 88.4 (2)°. In the crystal, adjacent mol­ecules are connected via pairs of N—H⋯S and C—H⋯O hydrogen bonds, which generate R (2) (2)(8) and R (2) (2)(10) graph-set motifs, respectively, resulting in a supra­molecular chain along the a axis.
format Online
Article
Text
id pubmed-3295489
institution National Center for Biotechnology Information
language English
publishDate 2012
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-32954892012-03-12 3-Benzyl-6-methyl-2-sulfanylidene-2,3-di­hydroquinazolin-4(1H)-one Al-Salahi, Rashad Al-Omar, Mohamed El-Subbagh, Hussein Hemamalini, Madhukar Fun, Hoong-Kun Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(16)H(14)N(2)OS, the quinazoline ring system is essentially planar, with a maximum deviation of 0.029 (3) Å. The dihedral angle between the quinazoline and benzene rings is 88.4 (2)°. In the crystal, adjacent mol­ecules are connected via pairs of N—H⋯S and C—H⋯O hydrogen bonds, which generate R (2) (2)(8) and R (2) (2)(10) graph-set motifs, respectively, resulting in a supra­molecular chain along the a axis. International Union of Crystallography 2012-02-17 /pmc/articles/PMC3295489/ /pubmed/22412600 http://dx.doi.org/10.1107/S1600536812006009 Text en © Al-Salahi et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Al-Salahi, Rashad
Al-Omar, Mohamed
El-Subbagh, Hussein
Hemamalini, Madhukar
Fun, Hoong-Kun
3-Benzyl-6-methyl-2-sulfanylidene-2,3-di­hydroquinazolin-4(1H)-one
title 3-Benzyl-6-methyl-2-sulfanylidene-2,3-di­hydroquinazolin-4(1H)-one
title_full 3-Benzyl-6-methyl-2-sulfanylidene-2,3-di­hydroquinazolin-4(1H)-one
title_fullStr 3-Benzyl-6-methyl-2-sulfanylidene-2,3-di­hydroquinazolin-4(1H)-one
title_full_unstemmed 3-Benzyl-6-methyl-2-sulfanylidene-2,3-di­hydroquinazolin-4(1H)-one
title_short 3-Benzyl-6-methyl-2-sulfanylidene-2,3-di­hydroquinazolin-4(1H)-one
title_sort 3-benzyl-6-methyl-2-sulfanylidene-2,3-di­hydroquinazolin-4(1h)-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3295489/
https://www.ncbi.nlm.nih.gov/pubmed/22412600
http://dx.doi.org/10.1107/S1600536812006009
work_keys_str_mv AT alsalahirashad 3benzyl6methyl2sulfanylidene23dihydroquinazolin41hone
AT alomarmohamed 3benzyl6methyl2sulfanylidene23dihydroquinazolin41hone
AT elsubbaghhussein 3benzyl6methyl2sulfanylidene23dihydroquinazolin41hone
AT hemamalinimadhukar 3benzyl6methyl2sulfanylidene23dihydroquinazolin41hone
AT funhoongkun 3benzyl6methyl2sulfanylidene23dihydroquinazolin41hone

Ejemplares similares