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4,4′-Bipyridine–2-methoxybenzoic acid (1/2)
The asymmetric unit of the title compound, C(10)H(8)N(2)·2C(8)H(8)O(3), contains two 2-methoxybenzoic acid molecules and one 4,4′-bipyridine molecule. The 4,4′-bipyridine molecule is disordered over two positions in a 1:1 ratio. In the crystal, the 2-methoxybenzoic acid and 4,4′-bipyridine mo...
Autores principales: | , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2012
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3297321/ https://www.ncbi.nlm.nih.gov/pubmed/22412511 http://dx.doi.org/10.1107/S1600536812003194 |
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author | Qian, Xiao-Yan Liu, Feng-Zhi |
author_facet | Qian, Xiao-Yan Liu, Feng-Zhi |
author_sort | Qian, Xiao-Yan |
collection | PubMed |
description | The asymmetric unit of the title compound, C(10)H(8)N(2)·2C(8)H(8)O(3), contains two 2-methoxybenzoic acid molecules and one 4,4′-bipyridine molecule. The 4,4′-bipyridine molecule is disordered over two positions in a 1:1 ratio. In the crystal, the 2-methoxybenzoic acid and 4,4′-bipyridine molecules are connected by intermolecular O—H⋯N hydrogen bonds. The dihedral angle between the carboxy group and its attached ring is 26.823 (2)°. |
format | Online Article Text |
id | pubmed-3297321 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2012 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-32973212012-03-12 4,4′-Bipyridine–2-methoxybenzoic acid (1/2) Qian, Xiao-Yan Liu, Feng-Zhi Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(10)H(8)N(2)·2C(8)H(8)O(3), contains two 2-methoxybenzoic acid molecules and one 4,4′-bipyridine molecule. The 4,4′-bipyridine molecule is disordered over two positions in a 1:1 ratio. In the crystal, the 2-methoxybenzoic acid and 4,4′-bipyridine molecules are connected by intermolecular O—H⋯N hydrogen bonds. The dihedral angle between the carboxy group and its attached ring is 26.823 (2)°. International Union of Crystallography 2012-02-04 /pmc/articles/PMC3297321/ /pubmed/22412511 http://dx.doi.org/10.1107/S1600536812003194 Text en © Qian and Liu 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Qian, Xiao-Yan Liu, Feng-Zhi 4,4′-Bipyridine–2-methoxybenzoic acid (1/2) |
title | 4,4′-Bipyridine–2-methoxybenzoic acid (1/2) |
title_full | 4,4′-Bipyridine–2-methoxybenzoic acid (1/2) |
title_fullStr | 4,4′-Bipyridine–2-methoxybenzoic acid (1/2) |
title_full_unstemmed | 4,4′-Bipyridine–2-methoxybenzoic acid (1/2) |
title_short | 4,4′-Bipyridine–2-methoxybenzoic acid (1/2) |
title_sort | 4,4′-bipyridine–2-methoxybenzoic acid (1/2) |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3297321/ https://www.ncbi.nlm.nih.gov/pubmed/22412511 http://dx.doi.org/10.1107/S1600536812003194 |
work_keys_str_mv | AT qianxiaoyan 44bipyridine2methoxybenzoicacid12 AT liufengzhi 44bipyridine2methoxybenzoicacid12 |