5,5′-[1,4-Phenyl­enebis(methyl­enesulfanedi­yl)]bis­[1,3,4-thia­diazol-2(3H)-one] dimethyl sulfoxide disolvate

The asymmetric unit of the title compound, C(12)H(10)N(4)O(2)S(4)·2C(2)H(6)OS, contains one half of the p-xylene mol­ecule and one dimethyl sulfoxide mol­ecule. The p-xylene mol­ecule is located about a crystallographic inversion centre. In the mol­ecule, the thia­diazole and benzene rings are almos...

Descripción completa

Detalles Bibliográficos
Autores principales: Kang, Sung Kwon, Cho, Nam Sook, Jang, Siyoung
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3297851/
https://www.ncbi.nlm.nih.gov/pubmed/22412654
http://dx.doi.org/10.1107/S1600536812006289
Descripción
Sumario:The asymmetric unit of the title compound, C(12)H(10)N(4)O(2)S(4)·2C(2)H(6)OS, contains one half of the p-xylene mol­ecule and one dimethyl sulfoxide mol­ecule. The p-xylene mol­ecule is located about a crystallographic inversion centre. In the mol­ecule, the thia­diazole and benzene rings are almost perpendicular to one another, with a dihedral angle of 88.95 (6)°. In the crystal, an N—H⋯O hydrogen bond is observed between the two components. The dimethyl sulfoxide mol­ecule is disordered over two orientations with an occupancy ratio of 0.879 (1):0.121 (1).

Ejemplares similares