2,4-Diiodo-6-[(propyl­imino)­meth­yl]phenol

The title compound, C(10)H(11)I(2)NO, was prepared by the reaction of 3,5-diiodo­salicyl­aldehyde with propyl­amine in ethanol. The mol­ecule adopts an E conformation with respect to the C=N bond and the aromatic ring. The aromatic ring and the imino unit are close to being coplanar, with a dihedral...

Descripción completa

Detalles Bibliográficos
Autores principales: Liu, Peng-Gang, Wang, Xiao-Ning, Yang, Yong-An, Zhu, Hai-Liang
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3297858/
https://www.ncbi.nlm.nih.gov/pubmed/22412661
http://dx.doi.org/10.1107/S1600536812005727
_version_ 1782225923405250560
author Liu, Peng-Gang
Wang, Xiao-Ning
Yang, Yong-An
Zhu, Hai-Liang
author_facet Liu, Peng-Gang
Wang, Xiao-Ning
Yang, Yong-An
Zhu, Hai-Liang
author_sort Liu, Peng-Gang
collection PubMed
description The title compound, C(10)H(11)I(2)NO, was prepared by the reaction of 3,5-diiodo­salicyl­aldehyde with propyl­amine in ethanol. The mol­ecule adopts an E conformation with respect to the C=N bond and the aromatic ring. The aromatic ring and the imino unit are close to being coplanar, with a dihedral angle of 2.6 (3)° between their planes. This planarity is assisted by the formation of an intra­molecular O—H⋯O hydrogen bond.
format Online
Article
Text
id pubmed-3297858
institution National Center for Biotechnology Information
language English
publishDate 2012
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-32978582012-03-12 2,4-Diiodo-6-[(propyl­imino)­meth­yl]phenol Liu, Peng-Gang Wang, Xiao-Ning Yang, Yong-An Zhu, Hai-Liang Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(10)H(11)I(2)NO, was prepared by the reaction of 3,5-diiodo­salicyl­aldehyde with propyl­amine in ethanol. The mol­ecule adopts an E conformation with respect to the C=N bond and the aromatic ring. The aromatic ring and the imino unit are close to being coplanar, with a dihedral angle of 2.6 (3)° between their planes. This planarity is assisted by the formation of an intra­molecular O—H⋯O hydrogen bond. International Union of Crystallography 2012-02-24 /pmc/articles/PMC3297858/ /pubmed/22412661 http://dx.doi.org/10.1107/S1600536812005727 Text en © Liu et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Liu, Peng-Gang
Wang, Xiao-Ning
Yang, Yong-An
Zhu, Hai-Liang
2,4-Diiodo-6-[(propyl­imino)­meth­yl]phenol
title 2,4-Diiodo-6-[(propyl­imino)­meth­yl]phenol
title_full 2,4-Diiodo-6-[(propyl­imino)­meth­yl]phenol
title_fullStr 2,4-Diiodo-6-[(propyl­imino)­meth­yl]phenol
title_full_unstemmed 2,4-Diiodo-6-[(propyl­imino)­meth­yl]phenol
title_short 2,4-Diiodo-6-[(propyl­imino)­meth­yl]phenol
title_sort 2,4-diiodo-6-[(propyl­imino)­meth­yl]phenol
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3297858/
https://www.ncbi.nlm.nih.gov/pubmed/22412661
http://dx.doi.org/10.1107/S1600536812005727
work_keys_str_mv AT liupenggang 24diiodo6propyliminomethylphenol
AT wangxiaoning 24diiodo6propyliminomethylphenol
AT yangyongan 24diiodo6propyliminomethylphenol
AT zhuhailiang 24diiodo6propyliminomethylphenol

Ejemplares similares