1-[(2-Hy­droxy­phen­yl)(pyrrolidin-1-yl)­meth­yl]naphthalen-2-ol N,N-dimethyl­formamide monosolvate

The title compound, C(21)H(21)NO(2)·C(3)H(7)NO, was synthesized by solvent-free one-pot three-component reaction of naphthalen-2-ol, 2-hy­droxy­benzaldehyde and pyrrolidine. The dihedral angle between the naphthalene ring system and the benzene ring is 77.74 (6)°. The pyrrolidine ring assumes an env...

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Autor principal: Wang, Wen-xiang
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3297932/
https://www.ncbi.nlm.nih.gov/pubmed/22412735
http://dx.doi.org/10.1107/S1600536812007787
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author Wang, Wen-xiang
author_facet Wang, Wen-xiang
author_sort Wang, Wen-xiang
collection PubMed
description The title compound, C(21)H(21)NO(2)·C(3)H(7)NO, was synthesized by solvent-free one-pot three-component reaction of naphthalen-2-ol, 2-hy­droxy­benzaldehyde and pyrrolidine. The dihedral angle between the naphthalene ring system and the benzene ring is 77.74 (6)°. The pyrrolidine ring assumes an envelope conformation. An intra­molecular O—H⋯N and an inter­molecular O—H⋯O hydrogen bond are observed.
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spelling pubmed-32979322012-03-12 1-[(2-Hy­droxy­phen­yl)(pyrrolidin-1-yl)­meth­yl]naphthalen-2-ol N,N-dimethyl­formamide monosolvate Wang, Wen-xiang Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(21)H(21)NO(2)·C(3)H(7)NO, was synthesized by solvent-free one-pot three-component reaction of naphthalen-2-ol, 2-hy­droxy­benzaldehyde and pyrrolidine. The dihedral angle between the naphthalene ring system and the benzene ring is 77.74 (6)°. The pyrrolidine ring assumes an envelope conformation. An intra­molecular O—H⋯N and an inter­molecular O—H⋯O hydrogen bond are observed. International Union of Crystallography 2012-02-29 /pmc/articles/PMC3297932/ /pubmed/22412735 http://dx.doi.org/10.1107/S1600536812007787 Text en © Wen-xiang Wang 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wang, Wen-xiang
1-[(2-Hy­droxy­phen­yl)(pyrrolidin-1-yl)­meth­yl]naphthalen-2-ol N,N-dimethyl­formamide monosolvate
title 1-[(2-Hy­droxy­phen­yl)(pyrrolidin-1-yl)­meth­yl]naphthalen-2-ol N,N-dimethyl­formamide monosolvate
title_full 1-[(2-Hy­droxy­phen­yl)(pyrrolidin-1-yl)­meth­yl]naphthalen-2-ol N,N-dimethyl­formamide monosolvate
title_fullStr 1-[(2-Hy­droxy­phen­yl)(pyrrolidin-1-yl)­meth­yl]naphthalen-2-ol N,N-dimethyl­formamide monosolvate
title_full_unstemmed 1-[(2-Hy­droxy­phen­yl)(pyrrolidin-1-yl)­meth­yl]naphthalen-2-ol N,N-dimethyl­formamide monosolvate
title_short 1-[(2-Hy­droxy­phen­yl)(pyrrolidin-1-yl)­meth­yl]naphthalen-2-ol N,N-dimethyl­formamide monosolvate
title_sort 1-[(2-hy­droxy­phen­yl)(pyrrolidin-1-yl)­meth­yl]naphthalen-2-ol n,n-dimethyl­formamide monosolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3297932/
https://www.ncbi.nlm.nih.gov/pubmed/22412735
http://dx.doi.org/10.1107/S1600536812007787
work_keys_str_mv AT wangwenxiang 12hydroxyphenylpyrrolidin1ylmethylnaphthalen2olnndimethylformamidemonosolvate

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