Cargando…

1,3-Bis{[(4-methyl­phen­yl)sulfon­yl]­oxy}propan-2-yl 4-methyl­benzene­sulfonate

In the title sulfonate derivative, C(24)H(26)O(9)S(3), all atoms apart from those of one of the 4-methyl­benzene­sulfonate residues lie approximately in a disc; the dihedral angles between the approximately orthogonal benzene ring and those in the plane are 74.53 (9) and 67.79 (11)°. In the crystal,...

Descripción completa

Detalles Bibliográficos
Autores principales: Yusof, Yusrabbil Amiyati, Ariffin, Azhar, Abu Hassan, Hazimah, Ng, Seik Weng, Tiekink, Edward R. T.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3297952/
https://www.ncbi.nlm.nih.gov/pubmed/22412755
http://dx.doi.org/10.1107/S1600536812008227
_version_ 1782225944951390208
author Yusof, Yusrabbil Amiyati
Ariffin, Azhar
Abu Hassan, Hazimah
Ng, Seik Weng
Tiekink, Edward R. T.
author_facet Yusof, Yusrabbil Amiyati
Ariffin, Azhar
Abu Hassan, Hazimah
Ng, Seik Weng
Tiekink, Edward R. T.
author_sort Yusof, Yusrabbil Amiyati
collection PubMed
description In the title sulfonate derivative, C(24)H(26)O(9)S(3), all atoms apart from those of one of the 4-methyl­benzene­sulfonate residues lie approximately in a disc; the dihedral angles between the approximately orthogonal benzene ring and those in the plane are 74.53 (9) and 67.79 (11)°. In the crystal, mol­ecules are consolidated into the three-dimensional architecture by C—H⋯O inter­actions. One of the 4-methyl­benzene­sulfonate residues is disordered over two almost parallel positions; the major component refined to a site-occupancy factor of 0.918 (2).
format Online
Article
Text
id pubmed-3297952
institution National Center for Biotechnology Information
language English
publishDate 2012
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-32979522012-03-12 1,3-Bis{[(4-methyl­phen­yl)sulfon­yl]­oxy}propan-2-yl 4-methyl­benzene­sulfonate Yusof, Yusrabbil Amiyati Ariffin, Azhar Abu Hassan, Hazimah Ng, Seik Weng Tiekink, Edward R. T. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title sulfonate derivative, C(24)H(26)O(9)S(3), all atoms apart from those of one of the 4-methyl­benzene­sulfonate residues lie approximately in a disc; the dihedral angles between the approximately orthogonal benzene ring and those in the plane are 74.53 (9) and 67.79 (11)°. In the crystal, mol­ecules are consolidated into the three-dimensional architecture by C—H⋯O inter­actions. One of the 4-methyl­benzene­sulfonate residues is disordered over two almost parallel positions; the major component refined to a site-occupancy factor of 0.918 (2). International Union of Crystallography 2012-02-29 /pmc/articles/PMC3297952/ /pubmed/22412755 http://dx.doi.org/10.1107/S1600536812008227 Text en © Yusof et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Yusof, Yusrabbil Amiyati
Ariffin, Azhar
Abu Hassan, Hazimah
Ng, Seik Weng
Tiekink, Edward R. T.
1,3-Bis{[(4-methyl­phen­yl)sulfon­yl]­oxy}propan-2-yl 4-methyl­benzene­sulfonate
title 1,3-Bis{[(4-methyl­phen­yl)sulfon­yl]­oxy}propan-2-yl 4-methyl­benzene­sulfonate
title_full 1,3-Bis{[(4-methyl­phen­yl)sulfon­yl]­oxy}propan-2-yl 4-methyl­benzene­sulfonate
title_fullStr 1,3-Bis{[(4-methyl­phen­yl)sulfon­yl]­oxy}propan-2-yl 4-methyl­benzene­sulfonate
title_full_unstemmed 1,3-Bis{[(4-methyl­phen­yl)sulfon­yl]­oxy}propan-2-yl 4-methyl­benzene­sulfonate
title_short 1,3-Bis{[(4-methyl­phen­yl)sulfon­yl]­oxy}propan-2-yl 4-methyl­benzene­sulfonate
title_sort 1,3-bis{[(4-methyl­phen­yl)sulfon­yl]­oxy}propan-2-yl 4-methyl­benzene­sulfonate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3297952/
https://www.ncbi.nlm.nih.gov/pubmed/22412755
http://dx.doi.org/10.1107/S1600536812008227
work_keys_str_mv AT yusofyusrabbilamiyati 13bis4methylphenylsulfonyloxypropan2yl4methylbenzenesulfonate
AT ariffinazhar 13bis4methylphenylsulfonyloxypropan2yl4methylbenzenesulfonate
AT abuhassanhazimah 13bis4methylphenylsulfonyloxypropan2yl4methylbenzenesulfonate
AT ngseikweng 13bis4methylphenylsulfonyloxypropan2yl4methylbenzenesulfonate
AT tiekinkedwardrt 13bis4methylphenylsulfonyloxypropan2yl4methylbenzenesulfonate