Cargando…
1,3-Bis{[(4-methylphenyl)sulfonyl]oxy}propan-2-yl 4-methylbenzenesulfonate
In the title sulfonate derivative, C(24)H(26)O(9)S(3), all atoms apart from those of one of the 4-methylbenzenesulfonate residues lie approximately in a disc; the dihedral angles between the approximately orthogonal benzene ring and those in the plane are 74.53 (9) and 67.79 (11)°. In the crystal,...
Autores principales: | , , , , |
---|---|
Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2012
|
Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3297952/ https://www.ncbi.nlm.nih.gov/pubmed/22412755 http://dx.doi.org/10.1107/S1600536812008227 |
_version_ | 1782225944951390208 |
---|---|
author | Yusof, Yusrabbil Amiyati Ariffin, Azhar Abu Hassan, Hazimah Ng, Seik Weng Tiekink, Edward R. T. |
author_facet | Yusof, Yusrabbil Amiyati Ariffin, Azhar Abu Hassan, Hazimah Ng, Seik Weng Tiekink, Edward R. T. |
author_sort | Yusof, Yusrabbil Amiyati |
collection | PubMed |
description | In the title sulfonate derivative, C(24)H(26)O(9)S(3), all atoms apart from those of one of the 4-methylbenzenesulfonate residues lie approximately in a disc; the dihedral angles between the approximately orthogonal benzene ring and those in the plane are 74.53 (9) and 67.79 (11)°. In the crystal, molecules are consolidated into the three-dimensional architecture by C—H⋯O interactions. One of the 4-methylbenzenesulfonate residues is disordered over two almost parallel positions; the major component refined to a site-occupancy factor of 0.918 (2). |
format | Online Article Text |
id | pubmed-3297952 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2012 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-32979522012-03-12 1,3-Bis{[(4-methylphenyl)sulfonyl]oxy}propan-2-yl 4-methylbenzenesulfonate Yusof, Yusrabbil Amiyati Ariffin, Azhar Abu Hassan, Hazimah Ng, Seik Weng Tiekink, Edward R. T. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title sulfonate derivative, C(24)H(26)O(9)S(3), all atoms apart from those of one of the 4-methylbenzenesulfonate residues lie approximately in a disc; the dihedral angles between the approximately orthogonal benzene ring and those in the plane are 74.53 (9) and 67.79 (11)°. In the crystal, molecules are consolidated into the three-dimensional architecture by C—H⋯O interactions. One of the 4-methylbenzenesulfonate residues is disordered over two almost parallel positions; the major component refined to a site-occupancy factor of 0.918 (2). International Union of Crystallography 2012-02-29 /pmc/articles/PMC3297952/ /pubmed/22412755 http://dx.doi.org/10.1107/S1600536812008227 Text en © Yusof et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Yusof, Yusrabbil Amiyati Ariffin, Azhar Abu Hassan, Hazimah Ng, Seik Weng Tiekink, Edward R. T. 1,3-Bis{[(4-methylphenyl)sulfonyl]oxy}propan-2-yl 4-methylbenzenesulfonate |
title | 1,3-Bis{[(4-methylphenyl)sulfonyl]oxy}propan-2-yl 4-methylbenzenesulfonate |
title_full | 1,3-Bis{[(4-methylphenyl)sulfonyl]oxy}propan-2-yl 4-methylbenzenesulfonate |
title_fullStr | 1,3-Bis{[(4-methylphenyl)sulfonyl]oxy}propan-2-yl 4-methylbenzenesulfonate |
title_full_unstemmed | 1,3-Bis{[(4-methylphenyl)sulfonyl]oxy}propan-2-yl 4-methylbenzenesulfonate |
title_short | 1,3-Bis{[(4-methylphenyl)sulfonyl]oxy}propan-2-yl 4-methylbenzenesulfonate |
title_sort | 1,3-bis{[(4-methylphenyl)sulfonyl]oxy}propan-2-yl 4-methylbenzenesulfonate |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3297952/ https://www.ncbi.nlm.nih.gov/pubmed/22412755 http://dx.doi.org/10.1107/S1600536812008227 |
work_keys_str_mv | AT yusofyusrabbilamiyati 13bis4methylphenylsulfonyloxypropan2yl4methylbenzenesulfonate AT ariffinazhar 13bis4methylphenylsulfonyloxypropan2yl4methylbenzenesulfonate AT abuhassanhazimah 13bis4methylphenylsulfonyloxypropan2yl4methylbenzenesulfonate AT ngseikweng 13bis4methylphenylsulfonyloxypropan2yl4methylbenzenesulfonate AT tiekinkedwardrt 13bis4methylphenylsulfonyloxypropan2yl4methylbenzenesulfonate |