4-[Bis(4-fluoro­phen­yl)meth­yl]piperazin-1-ium bis­(trichloro­acetate) 0.4-hydrate

The title compound, C(17)H(20)F(2)N(2) (2+)·2C(2)Cl(3)O(2) (−)·0.4H(2)O, has twofold protonated N atoms. The trichloro­acetate anions each show one disordered Cl atom with site occupation factors of 0.945 (7):0.055 (7) 0.945 (8):0.055 (8). In the crystal, N—H⋯O, O(water)—H⋯O and O(water)—H⋯F inter­a...

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Detalles Bibliográficos
Autores principales: Dayananda, A. S., Yathirajan, H. S., Flörke, Ulrich
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3343943/
https://www.ncbi.nlm.nih.gov/pubmed/22590024
http://dx.doi.org/10.1107/S1600536812009282
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author Dayananda, A. S.
Yathirajan, H. S.
Flörke, Ulrich
author_facet Dayananda, A. S.
Yathirajan, H. S.
Flörke, Ulrich
author_sort Dayananda, A. S.
collection PubMed
description The title compound, C(17)H(20)F(2)N(2) (2+)·2C(2)Cl(3)O(2) (−)·0.4H(2)O, has twofold protonated N atoms. The trichloro­acetate anions each show one disordered Cl atom with site occupation factors of 0.945 (7):0.055 (7) 0.945 (8):0.055 (8). In the crystal, N—H⋯O, O(water)—H⋯O and O(water)—H⋯F inter­actions connect the components into a three-dimensional network.
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spelling pubmed-33439432012-05-15 4-[Bis(4-fluoro­phen­yl)meth­yl]piperazin-1-ium bis­(trichloro­acetate) 0.4-hydrate Dayananda, A. S. Yathirajan, H. S. Flörke, Ulrich Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(17)H(20)F(2)N(2) (2+)·2C(2)Cl(3)O(2) (−)·0.4H(2)O, has twofold protonated N atoms. The trichloro­acetate anions each show one disordered Cl atom with site occupation factors of 0.945 (7):0.055 (7) 0.945 (8):0.055 (8). In the crystal, N—H⋯O, O(water)—H⋯O and O(water)—H⋯F inter­actions connect the components into a three-dimensional network. International Union of Crystallography 2012-03-07 /pmc/articles/PMC3343943/ /pubmed/22590024 http://dx.doi.org/10.1107/S1600536812009282 Text en © Dayananda et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Dayananda, A. S.
Yathirajan, H. S.
Flörke, Ulrich
4-[Bis(4-fluoro­phen­yl)meth­yl]piperazin-1-ium bis­(trichloro­acetate) 0.4-hydrate
title 4-[Bis(4-fluoro­phen­yl)meth­yl]piperazin-1-ium bis­(trichloro­acetate) 0.4-hydrate
title_full 4-[Bis(4-fluoro­phen­yl)meth­yl]piperazin-1-ium bis­(trichloro­acetate) 0.4-hydrate
title_fullStr 4-[Bis(4-fluoro­phen­yl)meth­yl]piperazin-1-ium bis­(trichloro­acetate) 0.4-hydrate
title_full_unstemmed 4-[Bis(4-fluoro­phen­yl)meth­yl]piperazin-1-ium bis­(trichloro­acetate) 0.4-hydrate
title_short 4-[Bis(4-fluoro­phen­yl)meth­yl]piperazin-1-ium bis­(trichloro­acetate) 0.4-hydrate
title_sort 4-[bis(4-fluoro­phen­yl)meth­yl]piperazin-1-ium bis­(trichloro­acetate) 0.4-hydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3343943/
https://www.ncbi.nlm.nih.gov/pubmed/22590024
http://dx.doi.org/10.1107/S1600536812009282
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