4-[3-(Biphenyl-4-yl)-1-phenyl-4,5-di­hydro-1H-pyrazol-5-yl]-3-(4-meth­oxy­phen­yl)-1-phenyl-1H-pyrazole dioxane monosolvate

In the title compound, C(37)H(30)N(4)O·C(4)H(8)O(2), the dihedral angle between the pyrazole and dihydro­pyrazole rings is 74.09 (10)°. In the crystal, the components are linked into centrosymmetric tetra­mers (two main mol­ecules and two solvent mol­ecules) by C—H⋯O hydrogen bonds. C—H⋯π and π–π [s...

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Detalles Bibliográficos
Autores principales: Fun, Hoong-Kun, Arshad, Suhana, Malladi, Shridhar, Isloor, Arun M., Shivananda, Kammasandra Nanjunda
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3343947/
https://www.ncbi.nlm.nih.gov/pubmed/22590028
http://dx.doi.org/10.1107/S1600536812009117
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author Fun, Hoong-Kun
Arshad, Suhana
Malladi, Shridhar
Isloor, Arun M.
Shivananda, Kammasandra Nanjunda
author_facet Fun, Hoong-Kun
Arshad, Suhana
Malladi, Shridhar
Isloor, Arun M.
Shivananda, Kammasandra Nanjunda
author_sort Fun, Hoong-Kun
collection PubMed
description In the title compound, C(37)H(30)N(4)O·C(4)H(8)O(2), the dihedral angle between the pyrazole and dihydro­pyrazole rings is 74.09 (10)°. In the crystal, the components are linked into centrosymmetric tetra­mers (two main mol­ecules and two solvent mol­ecules) by C—H⋯O hydrogen bonds. C—H⋯π and π–π [shortest centroid-centroid separation = 3.6546 (9) Å] inter­actions are also observed.
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spelling pubmed-33439472012-05-15 4-[3-(Biphenyl-4-yl)-1-phenyl-4,5-di­hydro-1H-pyrazol-5-yl]-3-(4-meth­oxy­phen­yl)-1-phenyl-1H-pyrazole dioxane monosolvate Fun, Hoong-Kun Arshad, Suhana Malladi, Shridhar Isloor, Arun M. Shivananda, Kammasandra Nanjunda Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(37)H(30)N(4)O·C(4)H(8)O(2), the dihedral angle between the pyrazole and dihydro­pyrazole rings is 74.09 (10)°. In the crystal, the components are linked into centrosymmetric tetra­mers (two main mol­ecules and two solvent mol­ecules) by C—H⋯O hydrogen bonds. C—H⋯π and π–π [shortest centroid-centroid separation = 3.6546 (9) Å] inter­actions are also observed. International Union of Crystallography 2012-03-07 /pmc/articles/PMC3343947/ /pubmed/22590028 http://dx.doi.org/10.1107/S1600536812009117 Text en © Fun et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Fun, Hoong-Kun
Arshad, Suhana
Malladi, Shridhar
Isloor, Arun M.
Shivananda, Kammasandra Nanjunda
4-[3-(Biphenyl-4-yl)-1-phenyl-4,5-di­hydro-1H-pyrazol-5-yl]-3-(4-meth­oxy­phen­yl)-1-phenyl-1H-pyrazole dioxane monosolvate
title 4-[3-(Biphenyl-4-yl)-1-phenyl-4,5-di­hydro-1H-pyrazol-5-yl]-3-(4-meth­oxy­phen­yl)-1-phenyl-1H-pyrazole dioxane monosolvate
title_full 4-[3-(Biphenyl-4-yl)-1-phenyl-4,5-di­hydro-1H-pyrazol-5-yl]-3-(4-meth­oxy­phen­yl)-1-phenyl-1H-pyrazole dioxane monosolvate
title_fullStr 4-[3-(Biphenyl-4-yl)-1-phenyl-4,5-di­hydro-1H-pyrazol-5-yl]-3-(4-meth­oxy­phen­yl)-1-phenyl-1H-pyrazole dioxane monosolvate
title_full_unstemmed 4-[3-(Biphenyl-4-yl)-1-phenyl-4,5-di­hydro-1H-pyrazol-5-yl]-3-(4-meth­oxy­phen­yl)-1-phenyl-1H-pyrazole dioxane monosolvate
title_short 4-[3-(Biphenyl-4-yl)-1-phenyl-4,5-di­hydro-1H-pyrazol-5-yl]-3-(4-meth­oxy­phen­yl)-1-phenyl-1H-pyrazole dioxane monosolvate
title_sort 4-[3-(biphenyl-4-yl)-1-phenyl-4,5-di­hydro-1h-pyrazol-5-yl]-3-(4-meth­oxy­phen­yl)-1-phenyl-1h-pyrazole dioxane monosolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3343947/
https://www.ncbi.nlm.nih.gov/pubmed/22590028
http://dx.doi.org/10.1107/S1600536812009117
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