1,4-Dihex­yloxy-2,5-bis­(2-nitro­phen­yl)benzene

The title compound, C(30)H(36)N(2)O(6), was prepared via twofold Suzuki coupling of a diboronic acid with bromo­nitro­benzene. The mol­ecule is located on a crystallographic inversion centre. The lateral benzene ring and the central ring make a dihedral angle of 48.75 (14)° and the nitro group is tw...

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Detalles Bibliográficos
Autores principales: Wrobel, Norma, Schollmeyer, Dieter, Detert, Heiner
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3343986/
https://www.ncbi.nlm.nih.gov/pubmed/22589895
http://dx.doi.org/10.1107/S1600536812009944
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author Wrobel, Norma
Schollmeyer, Dieter
Detert, Heiner
author_facet Wrobel, Norma
Schollmeyer, Dieter
Detert, Heiner
author_sort Wrobel, Norma
collection PubMed
description The title compound, C(30)H(36)N(2)O(6), was prepared via twofold Suzuki coupling of a diboronic acid with bromo­nitro­benzene. The mol­ecule is located on a crystallographic inversion centre. The lateral benzene ring and the central ring make a dihedral angle of 48.75 (14)° and the nitro group is twisted by 41.47 (13)° out of the plane of the benzene ring. The nitro and hex­yloxy groups are in close proximity and the hex­yloxy chain adopts an all-anti conformation.
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spelling pubmed-33439862012-05-15 1,4-Dihex­yloxy-2,5-bis­(2-nitro­phen­yl)benzene Wrobel, Norma Schollmeyer, Dieter Detert, Heiner Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(30)H(36)N(2)O(6), was prepared via twofold Suzuki coupling of a diboronic acid with bromo­nitro­benzene. The mol­ecule is located on a crystallographic inversion centre. The lateral benzene ring and the central ring make a dihedral angle of 48.75 (14)° and the nitro group is twisted by 41.47 (13)° out of the plane of the benzene ring. The nitro and hex­yloxy groups are in close proximity and the hex­yloxy chain adopts an all-anti conformation. International Union of Crystallography 2012-03-10 /pmc/articles/PMC3343986/ /pubmed/22589895 http://dx.doi.org/10.1107/S1600536812009944 Text en © Wrobel et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wrobel, Norma
Schollmeyer, Dieter
Detert, Heiner
1,4-Dihex­yloxy-2,5-bis­(2-nitro­phen­yl)benzene
title 1,4-Dihex­yloxy-2,5-bis­(2-nitro­phen­yl)benzene
title_full 1,4-Dihex­yloxy-2,5-bis­(2-nitro­phen­yl)benzene
title_fullStr 1,4-Dihex­yloxy-2,5-bis­(2-nitro­phen­yl)benzene
title_full_unstemmed 1,4-Dihex­yloxy-2,5-bis­(2-nitro­phen­yl)benzene
title_short 1,4-Dihex­yloxy-2,5-bis­(2-nitro­phen­yl)benzene
title_sort 1,4-dihex­yloxy-2,5-bis­(2-nitro­phen­yl)benzene
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3343986/
https://www.ncbi.nlm.nih.gov/pubmed/22589895
http://dx.doi.org/10.1107/S1600536812009944
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AT schollmeyerdieter 14dihexyloxy25bis2nitrophenylbenzene
AT detertheiner 14dihexyloxy25bis2nitrophenylbenzene

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