(E)-3-[(2-Hy­droxy-3-meth­oxy­benzyl­idene)amino]­benzoic acid

In the title compound, C(15)H(13)NO(4), the dihedral angle between the substituted benzene rings is 9.9 (8)°. Part of the mol­ecule (the salicylaldimine segment) is disordered over two sets of sites, with a refined site-occupancy ratio of 0.550 (14):0.450 (14). Intra­molecular O—H⋯N hydrogen bonds f...

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Autores principales: Kargar, Hadi, Sharafi, Zahra, Kia, Reza, Ghelenji, Safoora, Tahir, Muhammad Nawaz
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344025/
https://www.ncbi.nlm.nih.gov/pubmed/22589934
http://dx.doi.org/10.1107/S1600536812010549
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author Kargar, Hadi
Sharafi, Zahra
Kia, Reza
Ghelenji, Safoora
Tahir, Muhammad Nawaz
author_facet Kargar, Hadi
Sharafi, Zahra
Kia, Reza
Ghelenji, Safoora
Tahir, Muhammad Nawaz
author_sort Kargar, Hadi
collection PubMed
description In the title compound, C(15)H(13)NO(4), the dihedral angle between the substituted benzene rings is 9.9 (8)°. Part of the mol­ecule (the salicylaldimine segment) is disordered over two sets of sites, with a refined site-occupancy ratio of 0.550 (14):0.450 (14). Intra­molecular O—H⋯N hydrogen bonds form S(6) ring motifs. In the crystal, pairs of O—H⋯O hydrogen bonds link mol­ecules into centrosymmetric dimers with R (2) (2)(8) ring motifs. The crystal packing also features C—H⋯π inter­actions.
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spelling pubmed-33440252012-05-15 (E)-3-[(2-Hy­droxy-3-meth­oxy­benzyl­idene)amino]­benzoic acid Kargar, Hadi Sharafi, Zahra Kia, Reza Ghelenji, Safoora Tahir, Muhammad Nawaz Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(15)H(13)NO(4), the dihedral angle between the substituted benzene rings is 9.9 (8)°. Part of the mol­ecule (the salicylaldimine segment) is disordered over two sets of sites, with a refined site-occupancy ratio of 0.550 (14):0.450 (14). Intra­molecular O—H⋯N hydrogen bonds form S(6) ring motifs. In the crystal, pairs of O—H⋯O hydrogen bonds link mol­ecules into centrosymmetric dimers with R (2) (2)(8) ring motifs. The crystal packing also features C—H⋯π inter­actions. International Union of Crystallography 2012-03-14 /pmc/articles/PMC3344025/ /pubmed/22589934 http://dx.doi.org/10.1107/S1600536812010549 Text en © Kargar et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Kargar, Hadi
Sharafi, Zahra
Kia, Reza
Ghelenji, Safoora
Tahir, Muhammad Nawaz
(E)-3-[(2-Hy­droxy-3-meth­oxy­benzyl­idene)amino]­benzoic acid
title (E)-3-[(2-Hy­droxy-3-meth­oxy­benzyl­idene)amino]­benzoic acid
title_full (E)-3-[(2-Hy­droxy-3-meth­oxy­benzyl­idene)amino]­benzoic acid
title_fullStr (E)-3-[(2-Hy­droxy-3-meth­oxy­benzyl­idene)amino]­benzoic acid
title_full_unstemmed (E)-3-[(2-Hy­droxy-3-meth­oxy­benzyl­idene)amino]­benzoic acid
title_short (E)-3-[(2-Hy­droxy-3-meth­oxy­benzyl­idene)amino]­benzoic acid
title_sort (e)-3-[(2-hy­droxy-3-meth­oxy­benzyl­idene)amino]­benzoic acid
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344025/
https://www.ncbi.nlm.nih.gov/pubmed/22589934
http://dx.doi.org/10.1107/S1600536812010549
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