(E)-4-Bromo-N′-(4-hy­droxy-3-meth­oxy­benzyl­idene)benzohydrazide monohydrate

In the title compound, C(15)H(13)BrN(2)O(3)·H(2)O, the dihedral angle between the two benzene rings is 13.92 (6)°. The meth­oxy group of the 4-hy­droxy-3-meth­oxy­phenyl is almost coplanar with its bound benzene ring, as seen by the C(meth­yl)—O—C—C torsion angle of −0.35 (16)°. In the crystal, mol­...

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Autores principales: Horkaew, Jirapa, Chantrapromma, Suchada, Anantapong, Teerasak, Kanjana-Opas, Akkharawit, Fun, Hoong-Kun
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344027/
https://www.ncbi.nlm.nih.gov/pubmed/22589936
http://dx.doi.org/10.1107/S160053681201032X
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author Horkaew, Jirapa
Chantrapromma, Suchada
Anantapong, Teerasak
Kanjana-Opas, Akkharawit
Fun, Hoong-Kun
author_facet Horkaew, Jirapa
Chantrapromma, Suchada
Anantapong, Teerasak
Kanjana-Opas, Akkharawit
Fun, Hoong-Kun
author_sort Horkaew, Jirapa
collection PubMed
description In the title compound, C(15)H(13)BrN(2)O(3)·H(2)O, the dihedral angle between the two benzene rings is 13.92 (6)°. The meth­oxy group of the 4-hy­droxy-3-meth­oxy­phenyl is almost coplanar with its bound benzene ring, as seen by the C(meth­yl)—O—C—C torsion angle of −0.35 (16)°. In the crystal, mol­ecules are linked into a three-dimensional network by N—H⋯O, O—H⋯N and O—H⋯O hydrogen bonds and also weak C—H⋯O inter­actions. A short C⋯O contact of 3.0191 (15) Å is also present.
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spelling pubmed-33440272012-05-15 (E)-4-Bromo-N′-(4-hy­droxy-3-meth­oxy­benzyl­idene)benzohydrazide monohydrate Horkaew, Jirapa Chantrapromma, Suchada Anantapong, Teerasak Kanjana-Opas, Akkharawit Fun, Hoong-Kun Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(15)H(13)BrN(2)O(3)·H(2)O, the dihedral angle between the two benzene rings is 13.92 (6)°. The meth­oxy group of the 4-hy­droxy-3-meth­oxy­phenyl is almost coplanar with its bound benzene ring, as seen by the C(meth­yl)—O—C—C torsion angle of −0.35 (16)°. In the crystal, mol­ecules are linked into a three-dimensional network by N—H⋯O, O—H⋯N and O—H⋯O hydrogen bonds and also weak C—H⋯O inter­actions. A short C⋯O contact of 3.0191 (15) Å is also present. International Union of Crystallography 2012-03-14 /pmc/articles/PMC3344027/ /pubmed/22589936 http://dx.doi.org/10.1107/S160053681201032X Text en © Horkaew et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Horkaew, Jirapa
Chantrapromma, Suchada
Anantapong, Teerasak
Kanjana-Opas, Akkharawit
Fun, Hoong-Kun
(E)-4-Bromo-N′-(4-hy­droxy-3-meth­oxy­benzyl­idene)benzohydrazide monohydrate
title (E)-4-Bromo-N′-(4-hy­droxy-3-meth­oxy­benzyl­idene)benzohydrazide monohydrate
title_full (E)-4-Bromo-N′-(4-hy­droxy-3-meth­oxy­benzyl­idene)benzohydrazide monohydrate
title_fullStr (E)-4-Bromo-N′-(4-hy­droxy-3-meth­oxy­benzyl­idene)benzohydrazide monohydrate
title_full_unstemmed (E)-4-Bromo-N′-(4-hy­droxy-3-meth­oxy­benzyl­idene)benzohydrazide monohydrate
title_short (E)-4-Bromo-N′-(4-hy­droxy-3-meth­oxy­benzyl­idene)benzohydrazide monohydrate
title_sort (e)-4-bromo-n′-(4-hy­droxy-3-meth­oxy­benzyl­idene)benzohydrazide monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344027/
https://www.ncbi.nlm.nih.gov/pubmed/22589936
http://dx.doi.org/10.1107/S160053681201032X
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