4-[2-(Benzyl­amino)­phen­yl]-2,6-dimethyl­quinoline N-oxide

The title compound, C(24)H(22)N(2)O, was obtained in a two-step procedure from the corresponding 4-(2-iodo­phen­yl)quinoline. The quinoline system is approximately planar [maximum deviation from the least-squares plane = 0.021 (2) Å]. The planes of the quinoline system and the phenyl ring subtend a...

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Detalles Bibliográficos
Autores principales: Geffe, Mario, Schollmeyer, Dieter, Detert, Heiner
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344055/
https://www.ncbi.nlm.nih.gov/pubmed/22589964
http://dx.doi.org/10.1107/S1600536812011002
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author Geffe, Mario
Schollmeyer, Dieter
Detert, Heiner
author_facet Geffe, Mario
Schollmeyer, Dieter
Detert, Heiner
author_sort Geffe, Mario
collection PubMed
description The title compound, C(24)H(22)N(2)O, was obtained in a two-step procedure from the corresponding 4-(2-iodo­phen­yl)quinoline. The quinoline system is approximately planar [maximum deviation from the least-squares plane = 0.021 (2) Å]. The planes of the quinoline system and the phenyl ring subtend a dihedral angle of 78.08 (8)°. In the crystal, pairs of mol­ecules are connected via a center of symmetry and linked by a pair of angular N—H⋯O hydrogen bond. These dimers form columns oriented along the c axis.
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spelling pubmed-33440552012-05-15 4-[2-(Benzyl­amino)­phen­yl]-2,6-dimethyl­quinoline N-oxide Geffe, Mario Schollmeyer, Dieter Detert, Heiner Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(24)H(22)N(2)O, was obtained in a two-step procedure from the corresponding 4-(2-iodo­phen­yl)quinoline. The quinoline system is approximately planar [maximum deviation from the least-squares plane = 0.021 (2) Å]. The planes of the quinoline system and the phenyl ring subtend a dihedral angle of 78.08 (8)°. In the crystal, pairs of mol­ecules are connected via a center of symmetry and linked by a pair of angular N—H⋯O hydrogen bond. These dimers form columns oriented along the c axis. International Union of Crystallography 2012-03-17 /pmc/articles/PMC3344055/ /pubmed/22589964 http://dx.doi.org/10.1107/S1600536812011002 Text en © Geffe et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Geffe, Mario
Schollmeyer, Dieter
Detert, Heiner
4-[2-(Benzyl­amino)­phen­yl]-2,6-dimethyl­quinoline N-oxide
title 4-[2-(Benzyl­amino)­phen­yl]-2,6-dimethyl­quinoline N-oxide
title_full 4-[2-(Benzyl­amino)­phen­yl]-2,6-dimethyl­quinoline N-oxide
title_fullStr 4-[2-(Benzyl­amino)­phen­yl]-2,6-dimethyl­quinoline N-oxide
title_full_unstemmed 4-[2-(Benzyl­amino)­phen­yl]-2,6-dimethyl­quinoline N-oxide
title_short 4-[2-(Benzyl­amino)­phen­yl]-2,6-dimethyl­quinoline N-oxide
title_sort 4-[2-(benzyl­amino)­phen­yl]-2,6-dimethyl­quinoline n-oxide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344055/
https://www.ncbi.nlm.nih.gov/pubmed/22589964
http://dx.doi.org/10.1107/S1600536812011002
work_keys_str_mv AT geffemario 42benzylaminophenyl26dimethylquinolinenoxide
AT schollmeyerdieter 42benzylaminophenyl26dimethylquinolinenoxide
AT detertheiner 42benzylaminophenyl26dimethylquinolinenoxide

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