Cargando…
(E)-2-(2,3-Dimethylanilino)-N′-[2-methyl-5-(prop-1-en-2-yl)cyclohex-2-enylidene]benzohydrazide
The asymmetric unit of the title compound, C(25)H(29)N(3)O, comprises two crystallographically independent molecules. The dihedral angles between the benzene rings in the two molecules are 59.7 (2) and 61.27 (18)°. The cyclohexene rings adopt sofa and half-chair conformations. In the crystal, mol...
Autores principales: | , , , , |
---|---|
Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2012
|
Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344081/ https://www.ncbi.nlm.nih.gov/pubmed/22606084 http://dx.doi.org/10.1107/S1600536812009087 |
_version_ | 1782231911457882112 |
---|---|
author | Bhat, Mashooq A. Abdel-Aziz, Hatem A. Ghabbour, Hazem A. Hemamalini, Madhukar Fun, Hoong-Kun |
author_facet | Bhat, Mashooq A. Abdel-Aziz, Hatem A. Ghabbour, Hazem A. Hemamalini, Madhukar Fun, Hoong-Kun |
author_sort | Bhat, Mashooq A. |
collection | PubMed |
description | The asymmetric unit of the title compound, C(25)H(29)N(3)O, comprises two crystallographically independent molecules. The dihedral angles between the benzene rings in the two molecules are 59.7 (2) and 61.27 (18)°. The cyclohexene rings adopt sofa and half-chair conformations. In the crystal, molecules are connected via N—H⋯O and weak C—H⋯O hydrogen bonds, forming chains along the a axis. In each molecule, there is an intramolecular N—H⋯O hydrogen bond. |
format | Online Article Text |
id | pubmed-3344081 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2012 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-33440812012-05-17 (E)-2-(2,3-Dimethylanilino)-N′-[2-methyl-5-(prop-1-en-2-yl)cyclohex-2-enylidene]benzohydrazide Bhat, Mashooq A. Abdel-Aziz, Hatem A. Ghabbour, Hazem A. Hemamalini, Madhukar Fun, Hoong-Kun Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(25)H(29)N(3)O, comprises two crystallographically independent molecules. The dihedral angles between the benzene rings in the two molecules are 59.7 (2) and 61.27 (18)°. The cyclohexene rings adopt sofa and half-chair conformations. In the crystal, molecules are connected via N—H⋯O and weak C—H⋯O hydrogen bonds, forming chains along the a axis. In each molecule, there is an intramolecular N—H⋯O hydrogen bond. International Union of Crystallography 2012-03-21 /pmc/articles/PMC3344081/ /pubmed/22606084 http://dx.doi.org/10.1107/S1600536812009087 Text en © Bhat et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Bhat, Mashooq A. Abdel-Aziz, Hatem A. Ghabbour, Hazem A. Hemamalini, Madhukar Fun, Hoong-Kun (E)-2-(2,3-Dimethylanilino)-N′-[2-methyl-5-(prop-1-en-2-yl)cyclohex-2-enylidene]benzohydrazide |
title | (E)-2-(2,3-Dimethylanilino)-N′-[2-methyl-5-(prop-1-en-2-yl)cyclohex-2-enylidene]benzohydrazide |
title_full | (E)-2-(2,3-Dimethylanilino)-N′-[2-methyl-5-(prop-1-en-2-yl)cyclohex-2-enylidene]benzohydrazide |
title_fullStr | (E)-2-(2,3-Dimethylanilino)-N′-[2-methyl-5-(prop-1-en-2-yl)cyclohex-2-enylidene]benzohydrazide |
title_full_unstemmed | (E)-2-(2,3-Dimethylanilino)-N′-[2-methyl-5-(prop-1-en-2-yl)cyclohex-2-enylidene]benzohydrazide |
title_short | (E)-2-(2,3-Dimethylanilino)-N′-[2-methyl-5-(prop-1-en-2-yl)cyclohex-2-enylidene]benzohydrazide |
title_sort | (e)-2-(2,3-dimethylanilino)-n′-[2-methyl-5-(prop-1-en-2-yl)cyclohex-2-enylidene]benzohydrazide |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344081/ https://www.ncbi.nlm.nih.gov/pubmed/22606084 http://dx.doi.org/10.1107/S1600536812009087 |
work_keys_str_mv | AT bhatmashooqa e223dimethylanilinon2methyl5prop1en2ylcyclohex2enylidenebenzohydrazide AT abdelazizhatema e223dimethylanilinon2methyl5prop1en2ylcyclohex2enylidenebenzohydrazide AT ghabbourhazema e223dimethylanilinon2methyl5prop1en2ylcyclohex2enylidenebenzohydrazide AT hemamalinimadhukar e223dimethylanilinon2methyl5prop1en2ylcyclohex2enylidenebenzohydrazide AT funhoongkun e223dimethylanilinon2methyl5prop1en2ylcyclohex2enylidenebenzohydrazide |