3-Acetyl-1-(3-chloro­phen­yl)thio­urea

In the title compound, C(9)H(9)ClN(2)OS, the 3-chloro­phenyl and acetyl­thio­urea fragments are oriented at a dihedral angle of 62.68 (5)°. An intra­molecular N—H⋯O hydrogen bond generates an S(6) ring motif. Mol­ecules are linked into dimers via a cyclic R (2) (2)(8) motif of N—H⋯S hydrogen bonds....

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Detalles Bibliográficos
Autores principales: Shahwar, Durre, Tahir, M. Nawaz, Chohan, Muhammad Mansha, Ahmad, Naeem, Raza, M. Asam
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344126/
https://www.ncbi.nlm.nih.gov/pubmed/22606129
http://dx.doi.org/10.1107/S1600536812012147
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author Shahwar, Durre
Tahir, M. Nawaz
Chohan, Muhammad Mansha
Ahmad, Naeem
Raza, M. Asam
author_facet Shahwar, Durre
Tahir, M. Nawaz
Chohan, Muhammad Mansha
Ahmad, Naeem
Raza, M. Asam
author_sort Shahwar, Durre
collection PubMed
description In the title compound, C(9)H(9)ClN(2)OS, the 3-chloro­phenyl and acetyl­thio­urea fragments are oriented at a dihedral angle of 62.68 (5)°. An intra­molecular N—H⋯O hydrogen bond generates an S(6) ring motif. Mol­ecules are linked into dimers via a cyclic R (2) (2)(8) motif of N—H⋯S hydrogen bonds. These dimers are further connected through C—H⋯S inter­actions, completing an R (2) (2)(12) motif, into chains along [010].
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spelling pubmed-33441262012-05-17 3-Acetyl-1-(3-chloro­phen­yl)thio­urea Shahwar, Durre Tahir, M. Nawaz Chohan, Muhammad Mansha Ahmad, Naeem Raza, M. Asam Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(9)H(9)ClN(2)OS, the 3-chloro­phenyl and acetyl­thio­urea fragments are oriented at a dihedral angle of 62.68 (5)°. An intra­molecular N—H⋯O hydrogen bond generates an S(6) ring motif. Mol­ecules are linked into dimers via a cyclic R (2) (2)(8) motif of N—H⋯S hydrogen bonds. These dimers are further connected through C—H⋯S inter­actions, completing an R (2) (2)(12) motif, into chains along [010]. International Union of Crystallography 2012-03-24 /pmc/articles/PMC3344126/ /pubmed/22606129 http://dx.doi.org/10.1107/S1600536812012147 Text en © Shahwar et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Shahwar, Durre
Tahir, M. Nawaz
Chohan, Muhammad Mansha
Ahmad, Naeem
Raza, M. Asam
3-Acetyl-1-(3-chloro­phen­yl)thio­urea
title 3-Acetyl-1-(3-chloro­phen­yl)thio­urea
title_full 3-Acetyl-1-(3-chloro­phen­yl)thio­urea
title_fullStr 3-Acetyl-1-(3-chloro­phen­yl)thio­urea
title_full_unstemmed 3-Acetyl-1-(3-chloro­phen­yl)thio­urea
title_short 3-Acetyl-1-(3-chloro­phen­yl)thio­urea
title_sort 3-acetyl-1-(3-chloro­phen­yl)thio­urea
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344126/
https://www.ncbi.nlm.nih.gov/pubmed/22606129
http://dx.doi.org/10.1107/S1600536812012147
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AT tahirmnawaz 3acetyl13chlorophenylthiourea
AT chohanmuhammadmansha 3acetyl13chlorophenylthiourea
AT ahmadnaeem 3acetyl13chlorophenylthiourea
AT razamasam 3acetyl13chlorophenylthiourea

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