5-Nitro-1-(prop-2-yn-1-yl)-2,3-dihydro-1H-1,3-benzodiazol-2-one

In the two independent mol­ecules of the title compound, C(10)H(7)N(3)O(3), the nitro substitutent is twisted slightly with respect to the benzodiazol fused-ring system [dihedral angles = 4.9 (3) and 8.5 (1)°]. The two independent mol­ecules are disposed about a pseudo inversion center and are held...

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Detalles Bibliográficos
Autores principales: Ouzidan, Younes, Kandri Rodi, Youssef, Zouihri, Hafid, Essassi, El Mokhtar, Ng, Seik Weng
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344170/
https://www.ncbi.nlm.nih.gov/pubmed/22606173
http://dx.doi.org/10.1107/S1600536812013177
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author Ouzidan, Younes
Kandri Rodi, Youssef
Zouihri, Hafid
Essassi, El Mokhtar
Ng, Seik Weng
author_facet Ouzidan, Younes
Kandri Rodi, Youssef
Zouihri, Hafid
Essassi, El Mokhtar
Ng, Seik Weng
author_sort Ouzidan, Younes
collection PubMed
description In the two independent mol­ecules of the title compound, C(10)H(7)N(3)O(3), the nitro substitutent is twisted slightly with respect to the benzodiazol fused-ring system [dihedral angles = 4.9 (3) and 8.5 (1)°]. The two independent mol­ecules are disposed about a pseudo inversion center and are held together by N—H⋯O hydrogen bonds. The supramolecular dimer is essentially planar [dihedral angle between the fused rings = 2.0 (1)°]. Adjacent dimers are linked by acetyl­ene–nitro C—H⋯O inter­actions, generating a ribbon motif along (110).
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spelling pubmed-33441702012-05-17 5-Nitro-1-(prop-2-yn-1-yl)-2,3-dihydro-1H-1,3-benzodiazol-2-one Ouzidan, Younes Kandri Rodi, Youssef Zouihri, Hafid Essassi, El Mokhtar Ng, Seik Weng Acta Crystallogr Sect E Struct Rep Online Organic Papers In the two independent mol­ecules of the title compound, C(10)H(7)N(3)O(3), the nitro substitutent is twisted slightly with respect to the benzodiazol fused-ring system [dihedral angles = 4.9 (3) and 8.5 (1)°]. The two independent mol­ecules are disposed about a pseudo inversion center and are held together by N—H⋯O hydrogen bonds. The supramolecular dimer is essentially planar [dihedral angle between the fused rings = 2.0 (1)°]. Adjacent dimers are linked by acetyl­ene–nitro C—H⋯O inter­actions, generating a ribbon motif along (110). International Union of Crystallography 2012-03-31 /pmc/articles/PMC3344170/ /pubmed/22606173 http://dx.doi.org/10.1107/S1600536812013177 Text en © Ouzidan et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Ouzidan, Younes
Kandri Rodi, Youssef
Zouihri, Hafid
Essassi, El Mokhtar
Ng, Seik Weng
5-Nitro-1-(prop-2-yn-1-yl)-2,3-dihydro-1H-1,3-benzodiazol-2-one
title 5-Nitro-1-(prop-2-yn-1-yl)-2,3-dihydro-1H-1,3-benzodiazol-2-one
title_full 5-Nitro-1-(prop-2-yn-1-yl)-2,3-dihydro-1H-1,3-benzodiazol-2-one
title_fullStr 5-Nitro-1-(prop-2-yn-1-yl)-2,3-dihydro-1H-1,3-benzodiazol-2-one
title_full_unstemmed 5-Nitro-1-(prop-2-yn-1-yl)-2,3-dihydro-1H-1,3-benzodiazol-2-one
title_short 5-Nitro-1-(prop-2-yn-1-yl)-2,3-dihydro-1H-1,3-benzodiazol-2-one
title_sort 5-nitro-1-(prop-2-yn-1-yl)-2,3-dihydro-1h-1,3-benzodiazol-2-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344170/
https://www.ncbi.nlm.nih.gov/pubmed/22606173
http://dx.doi.org/10.1107/S1600536812013177
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