3,4-Dimeth­oxy-4′-nitro-1,1′-biphen­yl

The title compound, C(14)H(13)NO(4), was prepared through a palladium-catalysed Suzuki–Miyaura coupling reaction. The asymmetric unit comprises two mol­ecules related by pseudo-inversion symmetry. The dihedral angles between the benzene rings in the two mol­ecules are 44.30 (6) and 48.50 (6)° while...

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Detalles Bibliográficos
Autores principales: Li, Xin-Min, Hou, Yan-Jun, Chu, Wen-Yi, Sun, Zhi-Zhong
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344440/
https://www.ncbi.nlm.nih.gov/pubmed/22590202
http://dx.doi.org/10.1107/S1600536812013657
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author Li, Xin-Min
Hou, Yan-Jun
Chu, Wen-Yi
Sun, Zhi-Zhong
author_facet Li, Xin-Min
Hou, Yan-Jun
Chu, Wen-Yi
Sun, Zhi-Zhong
author_sort Li, Xin-Min
collection PubMed
description The title compound, C(14)H(13)NO(4), was prepared through a palladium-catalysed Suzuki–Miyaura coupling reaction. The asymmetric unit comprises two mol­ecules related by pseudo-inversion symmetry. The dihedral angles between the benzene rings in the two mol­ecules are 44.30 (6) and 48.50 (6)° while those between the benzene ring and the nitro group are 6.54 (13) and 5.73 (10)°. The crystal packing is defined only by Van der Waals inter­actions.
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spelling pubmed-33444402012-05-15 3,4-Dimeth­oxy-4′-nitro-1,1′-biphen­yl Li, Xin-Min Hou, Yan-Jun Chu, Wen-Yi Sun, Zhi-Zhong Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(14)H(13)NO(4), was prepared through a palladium-catalysed Suzuki–Miyaura coupling reaction. The asymmetric unit comprises two mol­ecules related by pseudo-inversion symmetry. The dihedral angles between the benzene rings in the two mol­ecules are 44.30 (6) and 48.50 (6)° while those between the benzene ring and the nitro group are 6.54 (13) and 5.73 (10)°. The crystal packing is defined only by Van der Waals inter­actions. International Union of Crystallography 2012-04-04 /pmc/articles/PMC3344440/ /pubmed/22590202 http://dx.doi.org/10.1107/S1600536812013657 Text en © Li et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Li, Xin-Min
Hou, Yan-Jun
Chu, Wen-Yi
Sun, Zhi-Zhong
3,4-Dimeth­oxy-4′-nitro-1,1′-biphen­yl
title 3,4-Dimeth­oxy-4′-nitro-1,1′-biphen­yl
title_full 3,4-Dimeth­oxy-4′-nitro-1,1′-biphen­yl
title_fullStr 3,4-Dimeth­oxy-4′-nitro-1,1′-biphen­yl
title_full_unstemmed 3,4-Dimeth­oxy-4′-nitro-1,1′-biphen­yl
title_short 3,4-Dimeth­oxy-4′-nitro-1,1′-biphen­yl
title_sort 3,4-dimeth­oxy-4′-nitro-1,1′-biphen­yl
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344440/
https://www.ncbi.nlm.nih.gov/pubmed/22590202
http://dx.doi.org/10.1107/S1600536812013657
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AT houyanjun 34dimethoxy4nitro11biphenyl
AT chuwenyi 34dimethoxy4nitro11biphenyl
AT sunzhizhong 34dimethoxy4nitro11biphenyl

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