2-[(3-Bromo­anilino)meth­yl]-1,2-benzo­thia­zol-3(2H)-one

The title compound, C(14)H(11)BrN(2)OS, was synthesized by the reaction of 1,2-benzothia­zol-3(2H)-one with formalin and 3-bromo­aniline in ethanol. The 1,2-benzothia­zolone ring system is approximately planar [maximum deviation = 0.0142 (s.u.?) Å] and forms a dihedral angle of 79.19 (5)° with the b...

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Detalles Bibliográficos
Autores principales: Wang, Xiang-Hui, Yang, Jian-Xin, Lin, Qiang, Chen, Jun-Hua
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344448/
https://www.ncbi.nlm.nih.gov/pubmed/22590210
http://dx.doi.org/10.1107/S1600536812012263
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author Wang, Xiang-Hui
Yang, Jian-Xin
Lin, Qiang
Chen, Jun-Hua
author_facet Wang, Xiang-Hui
Yang, Jian-Xin
Lin, Qiang
Chen, Jun-Hua
author_sort Wang, Xiang-Hui
collection PubMed
description The title compound, C(14)H(11)BrN(2)OS, was synthesized by the reaction of 1,2-benzothia­zol-3(2H)-one with formalin and 3-bromo­aniline in ethanol. The 1,2-benzothia­zolone ring system is approximately planar [maximum deviation = 0.0142 (s.u.?) Å] and forms a dihedral angle of 79.19 (5)° with the benzene ring. In the crystal, molecules are linked by N—H⋯O, C—H⋯O and C—H⋯Br interactions.
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spelling pubmed-33444482012-05-15 2-[(3-Bromo­anilino)meth­yl]-1,2-benzo­thia­zol-3(2H)-one Wang, Xiang-Hui Yang, Jian-Xin Lin, Qiang Chen, Jun-Hua Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(14)H(11)BrN(2)OS, was synthesized by the reaction of 1,2-benzothia­zol-3(2H)-one with formalin and 3-bromo­aniline in ethanol. The 1,2-benzothia­zolone ring system is approximately planar [maximum deviation = 0.0142 (s.u.?) Å] and forms a dihedral angle of 79.19 (5)° with the benzene ring. In the crystal, molecules are linked by N—H⋯O, C—H⋯O and C—H⋯Br interactions. International Union of Crystallography 2012-04-04 /pmc/articles/PMC3344448/ /pubmed/22590210 http://dx.doi.org/10.1107/S1600536812012263 Text en © Wang et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wang, Xiang-Hui
Yang, Jian-Xin
Lin, Qiang
Chen, Jun-Hua
2-[(3-Bromo­anilino)meth­yl]-1,2-benzo­thia­zol-3(2H)-one
title 2-[(3-Bromo­anilino)meth­yl]-1,2-benzo­thia­zol-3(2H)-one
title_full 2-[(3-Bromo­anilino)meth­yl]-1,2-benzo­thia­zol-3(2H)-one
title_fullStr 2-[(3-Bromo­anilino)meth­yl]-1,2-benzo­thia­zol-3(2H)-one
title_full_unstemmed 2-[(3-Bromo­anilino)meth­yl]-1,2-benzo­thia­zol-3(2H)-one
title_short 2-[(3-Bromo­anilino)meth­yl]-1,2-benzo­thia­zol-3(2H)-one
title_sort 2-[(3-bromo­anilino)meth­yl]-1,2-benzo­thia­zol-3(2h)-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344448/
https://www.ncbi.nlm.nih.gov/pubmed/22590210
http://dx.doi.org/10.1107/S1600536812012263
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AT chenjunhua 23bromoanilinomethyl12benzothiazol32hone

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