(E)-N′-(5-Bromo-2-hy­droxy­benzyl­idene)-4-(dimethyl­amino)­benzohydrazide

The title compound, C(16)H(16)BrN(3)O(2), crystallized with two independent molcules in the asymmetric unit. Each mol­ecule has an E conformation about the C=N bond and the dihedral angles between the benzene rings are 30.5 (3) and 28.7 (3)°. In each mol­ecule, there is an O—H⋯N hydrogen bond and th...

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Detalles Bibliográficos
Autor principal: Wei, En-Yu
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344449/
https://www.ncbi.nlm.nih.gov/pubmed/22590211
http://dx.doi.org/10.1107/S1600536812013785
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author Wei, En-Yu
author_facet Wei, En-Yu
author_sort Wei, En-Yu
collection PubMed
description The title compound, C(16)H(16)BrN(3)O(2), crystallized with two independent molcules in the asymmetric unit. Each mol­ecule has an E conformation about the C=N bond and the dihedral angles between the benzene rings are 30.5 (3) and 28.7 (3)°. In each mol­ecule, there is an O—H⋯N hydrogen bond and the two mol­ecules are linked by an N—H⋯O hydrogen bond. In the crystal, mol­ecules are further linked via N—H⋯O hydrogen bonds into chains propagating along [001].
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spelling pubmed-33444492012-05-15 (E)-N′-(5-Bromo-2-hy­droxy­benzyl­idene)-4-(dimethyl­amino)­benzohydrazide Wei, En-Yu Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(16)H(16)BrN(3)O(2), crystallized with two independent molcules in the asymmetric unit. Each mol­ecule has an E conformation about the C=N bond and the dihedral angles between the benzene rings are 30.5 (3) and 28.7 (3)°. In each mol­ecule, there is an O—H⋯N hydrogen bond and the two mol­ecules are linked by an N—H⋯O hydrogen bond. In the crystal, mol­ecules are further linked via N—H⋯O hydrogen bonds into chains propagating along [001]. International Union of Crystallography 2012-04-04 /pmc/articles/PMC3344449/ /pubmed/22590211 http://dx.doi.org/10.1107/S1600536812013785 Text en © En-Yu Wei 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wei, En-Yu
(E)-N′-(5-Bromo-2-hy­droxy­benzyl­idene)-4-(dimethyl­amino)­benzohydrazide
title (E)-N′-(5-Bromo-2-hy­droxy­benzyl­idene)-4-(dimethyl­amino)­benzohydrazide
title_full (E)-N′-(5-Bromo-2-hy­droxy­benzyl­idene)-4-(dimethyl­amino)­benzohydrazide
title_fullStr (E)-N′-(5-Bromo-2-hy­droxy­benzyl­idene)-4-(dimethyl­amino)­benzohydrazide
title_full_unstemmed (E)-N′-(5-Bromo-2-hy­droxy­benzyl­idene)-4-(dimethyl­amino)­benzohydrazide
title_short (E)-N′-(5-Bromo-2-hy­droxy­benzyl­idene)-4-(dimethyl­amino)­benzohydrazide
title_sort (e)-n′-(5-bromo-2-hy­droxy­benzyl­idene)-4-(dimethyl­amino)­benzohydrazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344449/
https://www.ncbi.nlm.nih.gov/pubmed/22590211
http://dx.doi.org/10.1107/S1600536812013785
work_keys_str_mv AT weienyu en5bromo2hydroxybenzylidene4dimethylaminobenzohydrazide

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