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Resorcinol ninhydrin complex: 1,5,9-trihydroxy-8-oxatetracyclo[7.7.0.0(2,7).0(10,15)]hexadeca-2,4,6,10(15),11,13-hexaen-16-one
In the title compound, C(15)H(10)O(5), the cyclopentanone (r.m.s. deviation = 0.049 Å) and oxolane (r.m.s. deviation = 0.048 Å) rings make a dihedral angle of 67.91 (4)°. An intramolecular O—H⋯O hydrogen bond is observed. In the crystal, molecules associate via O—H⋯O hydrogen bonds, forming a th...
| Autores principales: | , , , , |
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| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
International Union of Crystallography
2012
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| Materias: | |
| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344462/ https://www.ncbi.nlm.nih.gov/pubmed/22590224 http://dx.doi.org/10.1107/S1600536812014249 |
| _version_ | 1782231997241884672 |
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| author | Devi, T. Uma Priya, S. Kalpana, G. Selvanayagam, S. Sridhar, B. |
| author_facet | Devi, T. Uma Priya, S. Kalpana, G. Selvanayagam, S. Sridhar, B. |
| author_sort | Devi, T. Uma |
| collection | PubMed |
| description | In the title compound, C(15)H(10)O(5), the cyclopentanone (r.m.s. deviation = 0.049 Å) and oxolane (r.m.s. deviation = 0.048 Å) rings make a dihedral angle of 67.91 (4)°. An intramolecular O—H⋯O hydrogen bond is observed. In the crystal, molecules associate via O—H⋯O hydrogen bonds, forming a three-dimensional network. |
| format | Online Article Text |
| id | pubmed-3344462 |
| institution | National Center for Biotechnology Information |
| language | English |
| publishDate | 2012 |
| publisher | International Union of Crystallography |
| record_format | MEDLINE/PubMed |
| spelling | pubmed-33444622012-05-15 Resorcinol ninhydrin complex: 1,5,9-trihydroxy-8-oxatetracyclo[7.7.0.0(2,7).0(10,15)]hexadeca-2,4,6,10(15),11,13-hexaen-16-one Devi, T. Uma Priya, S. Kalpana, G. Selvanayagam, S. Sridhar, B. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(15)H(10)O(5), the cyclopentanone (r.m.s. deviation = 0.049 Å) and oxolane (r.m.s. deviation = 0.048 Å) rings make a dihedral angle of 67.91 (4)°. An intramolecular O—H⋯O hydrogen bond is observed. In the crystal, molecules associate via O—H⋯O hydrogen bonds, forming a three-dimensional network. International Union of Crystallography 2012-04-06 /pmc/articles/PMC3344462/ /pubmed/22590224 http://dx.doi.org/10.1107/S1600536812014249 Text en © Devi et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
| spellingShingle | Organic Papers Devi, T. Uma Priya, S. Kalpana, G. Selvanayagam, S. Sridhar, B. Resorcinol ninhydrin complex: 1,5,9-trihydroxy-8-oxatetracyclo[7.7.0.0(2,7).0(10,15)]hexadeca-2,4,6,10(15),11,13-hexaen-16-one |
| title | Resorcinol ninhydrin complex: 1,5,9-trihydroxy-8-oxatetracyclo[7.7.0.0(2,7).0(10,15)]hexadeca-2,4,6,10(15),11,13-hexaen-16-one |
| title_full | Resorcinol ninhydrin complex: 1,5,9-trihydroxy-8-oxatetracyclo[7.7.0.0(2,7).0(10,15)]hexadeca-2,4,6,10(15),11,13-hexaen-16-one |
| title_fullStr | Resorcinol ninhydrin complex: 1,5,9-trihydroxy-8-oxatetracyclo[7.7.0.0(2,7).0(10,15)]hexadeca-2,4,6,10(15),11,13-hexaen-16-one |
| title_full_unstemmed | Resorcinol ninhydrin complex: 1,5,9-trihydroxy-8-oxatetracyclo[7.7.0.0(2,7).0(10,15)]hexadeca-2,4,6,10(15),11,13-hexaen-16-one |
| title_short | Resorcinol ninhydrin complex: 1,5,9-trihydroxy-8-oxatetracyclo[7.7.0.0(2,7).0(10,15)]hexadeca-2,4,6,10(15),11,13-hexaen-16-one |
| title_sort | resorcinol ninhydrin complex: 1,5,9-trihydroxy-8-oxatetracyclo[7.7.0.0(2,7).0(10,15)]hexadeca-2,4,6,10(15),11,13-hexaen-16-one |
| topic | Organic Papers |
| url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344462/ https://www.ncbi.nlm.nih.gov/pubmed/22590224 http://dx.doi.org/10.1107/S1600536812014249 |
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