(1RS,2SR,5SR)-9-Benzyl-2-[(1RS)-1-hy­droxy­benz­yl]-9-aza­bicyclo­[3.3.1]nonan-3-one from synchrotron data

In the crystal structure of the racemic title compound, C(22)H(25)NO(2), solved and refined against sychrotron diffraction data, the hy­droxy group and the carbonyl O atom participate in the formation of O—H⋯O hydrogen bonds between pairs of enanti­omers related by a crystallographic centre of symme...

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Autores principales: Lazny, Ryszard, Wolosewicz, Karol, Dauter, Zbigniew, Brzezinski, Krzysztof
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344499/
https://www.ncbi.nlm.nih.gov/pubmed/22590261
http://dx.doi.org/10.1107/S1600536812014754
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author Lazny, Ryszard
Wolosewicz, Karol
Dauter, Zbigniew
Brzezinski, Krzysztof
author_facet Lazny, Ryszard
Wolosewicz, Karol
Dauter, Zbigniew
Brzezinski, Krzysztof
author_sort Lazny, Ryszard
collection PubMed
description In the crystal structure of the racemic title compound, C(22)H(25)NO(2), solved and refined against sychrotron diffraction data, the hy­droxy group and the carbonyl O atom participate in the formation of O—H⋯O hydrogen bonds between pairs of enanti­omers related by a crystallographic centre of symmetry.
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spelling pubmed-33444992012-05-15 (1RS,2SR,5SR)-9-Benzyl-2-[(1RS)-1-hy­droxy­benz­yl]-9-aza­bicyclo­[3.3.1]nonan-3-one from synchrotron data Lazny, Ryszard Wolosewicz, Karol Dauter, Zbigniew Brzezinski, Krzysztof Acta Crystallogr Sect E Struct Rep Online Organic Papers In the crystal structure of the racemic title compound, C(22)H(25)NO(2), solved and refined against sychrotron diffraction data, the hy­droxy group and the carbonyl O atom participate in the formation of O—H⋯O hydrogen bonds between pairs of enanti­omers related by a crystallographic centre of symmetry. International Union of Crystallography 2012-04-13 /pmc/articles/PMC3344499/ /pubmed/22590261 http://dx.doi.org/10.1107/S1600536812014754 Text en © Lazny et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Lazny, Ryszard
Wolosewicz, Karol
Dauter, Zbigniew
Brzezinski, Krzysztof
(1RS,2SR,5SR)-9-Benzyl-2-[(1RS)-1-hy­droxy­benz­yl]-9-aza­bicyclo­[3.3.1]nonan-3-one from synchrotron data
title (1RS,2SR,5SR)-9-Benzyl-2-[(1RS)-1-hy­droxy­benz­yl]-9-aza­bicyclo­[3.3.1]nonan-3-one from synchrotron data
title_full (1RS,2SR,5SR)-9-Benzyl-2-[(1RS)-1-hy­droxy­benz­yl]-9-aza­bicyclo­[3.3.1]nonan-3-one from synchrotron data
title_fullStr (1RS,2SR,5SR)-9-Benzyl-2-[(1RS)-1-hy­droxy­benz­yl]-9-aza­bicyclo­[3.3.1]nonan-3-one from synchrotron data
title_full_unstemmed (1RS,2SR,5SR)-9-Benzyl-2-[(1RS)-1-hy­droxy­benz­yl]-9-aza­bicyclo­[3.3.1]nonan-3-one from synchrotron data
title_short (1RS,2SR,5SR)-9-Benzyl-2-[(1RS)-1-hy­droxy­benz­yl]-9-aza­bicyclo­[3.3.1]nonan-3-one from synchrotron data
title_sort (1rs,2sr,5sr)-9-benzyl-2-[(1rs)-1-hy­droxy­benz­yl]-9-aza­bicyclo­[3.3.1]nonan-3-one from synchrotron data
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344499/
https://www.ncbi.nlm.nih.gov/pubmed/22590261
http://dx.doi.org/10.1107/S1600536812014754
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