11-(4-Meth­oxy­phen­yl)-3,3-dimethyl-2,3,4,5,10,11-hexa­hydro-1H-dibenzo[b,e][1,4]diazepin-1-one monohydrate

In the title compound, C(22)H(24)N(2)O(2)·H(2)O, the co-crystallized water mol­ecule inter­acts with the N and O atoms of the mol­ecule through O(w)—H⋯N, O(w)—H⋯O(meth­yl) and N—H⋯O(w) hydrogen-bonding inter­actions. These hydrogen bonds, along with the inter­molecular N—H⋯O=C hydrogen-bonding inter...

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Autores principales: Fadare, Olatomide A., Adelani, Pius O., Ikotun, Adebomi A., Obafemi, Craig A.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344616/
https://www.ncbi.nlm.nih.gov/pubmed/22590378
http://dx.doi.org/10.1107/S1600536812016194
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author Fadare, Olatomide A.
Adelani, Pius O.
Ikotun, Adebomi A.
Obafemi, Craig A.
author_facet Fadare, Olatomide A.
Adelani, Pius O.
Ikotun, Adebomi A.
Obafemi, Craig A.
author_sort Fadare, Olatomide A.
collection PubMed
description In the title compound, C(22)H(24)N(2)O(2)·H(2)O, the co-crystallized water mol­ecule inter­acts with the N and O atoms of the mol­ecule through O(w)—H⋯N, O(w)—H⋯O(meth­yl) and N—H⋯O(w) hydrogen-bonding inter­actions. These hydrogen bonds, along with the inter­molecular N—H⋯O=C hydrogen-bonding inter­actions, connect the mol­ecules into a three-dimensional network. The dihedral angle between the two aromatic rings is 65.46 (10)°.
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spelling pubmed-33446162012-05-15 11-(4-Meth­oxy­phen­yl)-3,3-dimethyl-2,3,4,5,10,11-hexa­hydro-1H-dibenzo[b,e][1,4]diazepin-1-one monohydrate Fadare, Olatomide A. Adelani, Pius O. Ikotun, Adebomi A. Obafemi, Craig A. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(22)H(24)N(2)O(2)·H(2)O, the co-crystallized water mol­ecule inter­acts with the N and O atoms of the mol­ecule through O(w)—H⋯N, O(w)—H⋯O(meth­yl) and N—H⋯O(w) hydrogen-bonding inter­actions. These hydrogen bonds, along with the inter­molecular N—H⋯O=C hydrogen-bonding inter­actions, connect the mol­ecules into a three-dimensional network. The dihedral angle between the two aromatic rings is 65.46 (10)°. International Union of Crystallography 2012-04-25 /pmc/articles/PMC3344616/ /pubmed/22590378 http://dx.doi.org/10.1107/S1600536812016194 Text en © Fadare et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Fadare, Olatomide A.
Adelani, Pius O.
Ikotun, Adebomi A.
Obafemi, Craig A.
11-(4-Meth­oxy­phen­yl)-3,3-dimethyl-2,3,4,5,10,11-hexa­hydro-1H-dibenzo[b,e][1,4]diazepin-1-one monohydrate
title 11-(4-Meth­oxy­phen­yl)-3,3-dimethyl-2,3,4,5,10,11-hexa­hydro-1H-dibenzo[b,e][1,4]diazepin-1-one monohydrate
title_full 11-(4-Meth­oxy­phen­yl)-3,3-dimethyl-2,3,4,5,10,11-hexa­hydro-1H-dibenzo[b,e][1,4]diazepin-1-one monohydrate
title_fullStr 11-(4-Meth­oxy­phen­yl)-3,3-dimethyl-2,3,4,5,10,11-hexa­hydro-1H-dibenzo[b,e][1,4]diazepin-1-one monohydrate
title_full_unstemmed 11-(4-Meth­oxy­phen­yl)-3,3-dimethyl-2,3,4,5,10,11-hexa­hydro-1H-dibenzo[b,e][1,4]diazepin-1-one monohydrate
title_short 11-(4-Meth­oxy­phen­yl)-3,3-dimethyl-2,3,4,5,10,11-hexa­hydro-1H-dibenzo[b,e][1,4]diazepin-1-one monohydrate
title_sort 11-(4-meth­oxy­phen­yl)-3,3-dimethyl-2,3,4,5,10,11-hexa­hydro-1h-dibenzo[b,e][1,4]diazepin-1-one monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344616/
https://www.ncbi.nlm.nih.gov/pubmed/22590378
http://dx.doi.org/10.1107/S1600536812016194
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