(E)-N′-[3-(4-Chloro­benzo­yloxy)benzyl­idene]pyridine-4-carbohydrazide acetic acid monosolvate monohydrate

In the Schiff base mol­ecule of the title compound, C(20)H(14)ClN(3)O(3)·CH(3)COOH·H(2)O, the central benzene ring makes dihedral angles of 36.26 (7) and 27.59 (8)°, respectively, with the terminal chloro­phenyl and pyridine rings. In the crystal, the three components are linked by O—H⋯O, N—H⋯O, O—H...

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Detalles Bibliográficos
Autores principales: Diao, Chun-Hua, Fan, Zhi
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344622/
https://www.ncbi.nlm.nih.gov/pubmed/22590384
http://dx.doi.org/10.1107/S1600536812017369
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author Diao, Chun-Hua
Fan, Zhi
author_facet Diao, Chun-Hua
Fan, Zhi
author_sort Diao, Chun-Hua
collection PubMed
description In the Schiff base mol­ecule of the title compound, C(20)H(14)ClN(3)O(3)·CH(3)COOH·H(2)O, the central benzene ring makes dihedral angles of 36.26 (7) and 27.59 (8)°, respectively, with the terminal chloro­phenyl and pyridine rings. In the crystal, the three components are linked by O—H⋯O, N—H⋯O, O—H⋯N and C—H⋯O hydrogen bonds into a double-tape structure along the a axis.
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spelling pubmed-33446222012-05-15 (E)-N′-[3-(4-Chloro­benzo­yloxy)benzyl­idene]pyridine-4-carbohydrazide acetic acid monosolvate monohydrate Diao, Chun-Hua Fan, Zhi Acta Crystallogr Sect E Struct Rep Online Organic Papers In the Schiff base mol­ecule of the title compound, C(20)H(14)ClN(3)O(3)·CH(3)COOH·H(2)O, the central benzene ring makes dihedral angles of 36.26 (7) and 27.59 (8)°, respectively, with the terminal chloro­phenyl and pyridine rings. In the crystal, the three components are linked by O—H⋯O, N—H⋯O, O—H⋯N and C—H⋯O hydrogen bonds into a double-tape structure along the a axis. International Union of Crystallography 2012-04-25 /pmc/articles/PMC3344622/ /pubmed/22590384 http://dx.doi.org/10.1107/S1600536812017369 Text en © Diao and Fan 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Diao, Chun-Hua
Fan, Zhi
(E)-N′-[3-(4-Chloro­benzo­yloxy)benzyl­idene]pyridine-4-carbohydrazide acetic acid monosolvate monohydrate
title (E)-N′-[3-(4-Chloro­benzo­yloxy)benzyl­idene]pyridine-4-carbohydrazide acetic acid monosolvate monohydrate
title_full (E)-N′-[3-(4-Chloro­benzo­yloxy)benzyl­idene]pyridine-4-carbohydrazide acetic acid monosolvate monohydrate
title_fullStr (E)-N′-[3-(4-Chloro­benzo­yloxy)benzyl­idene]pyridine-4-carbohydrazide acetic acid monosolvate monohydrate
title_full_unstemmed (E)-N′-[3-(4-Chloro­benzo­yloxy)benzyl­idene]pyridine-4-carbohydrazide acetic acid monosolvate monohydrate
title_short (E)-N′-[3-(4-Chloro­benzo­yloxy)benzyl­idene]pyridine-4-carbohydrazide acetic acid monosolvate monohydrate
title_sort (e)-n′-[3-(4-chloro­benzo­yloxy)benzyl­idene]pyridine-4-carbohydrazide acetic acid monosolvate monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344622/
https://www.ncbi.nlm.nih.gov/pubmed/22590384
http://dx.doi.org/10.1107/S1600536812017369
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AT fanzhi en34chlorobenzoyloxybenzylidenepyridine4carbohydrazideaceticacidmonosolvatemonohydrate

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