1-(4-Chloro­butano­yl)-3-(2-chloro­phen­yl)thio­urea

The asymmetric unit of the title compound, C(11)H(12)Cl(2)N(2)OS, contains two crystallographically independent mol­ecules with different conformations: the benzene ring and the thio­urea fragment form dihedral angles of 74.32 (11) and 89.39 (11)°. One amino group in each mol­ecule is involved in in...

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Autores principales: Yusof, M. Sukeri M., Embong, Nur Farhana, Yamin, Bohari M., Ngah, Nurziana
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344638/
https://www.ncbi.nlm.nih.gov/pubmed/22590400
http://dx.doi.org/10.1107/S160053681201759X
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author Yusof, M. Sukeri M.
Embong, Nur Farhana
Yamin, Bohari M.
Ngah, Nurziana
author_facet Yusof, M. Sukeri M.
Embong, Nur Farhana
Yamin, Bohari M.
Ngah, Nurziana
author_sort Yusof, M. Sukeri M.
collection PubMed
description The asymmetric unit of the title compound, C(11)H(12)Cl(2)N(2)OS, contains two crystallographically independent mol­ecules with different conformations: the benzene ring and the thio­urea fragment form dihedral angles of 74.32 (11) and 89.39 (11)°. One amino group in each mol­ecule is involved in intra­molecular N—H⋯O and inter­molecular N—H⋯O hydrogen bonding: the latter links pairs of independent mol­ecules into dimers. In the crystal, weak N—H⋯S inter­actions link these dimers into chains propagating along the c axis.
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spelling pubmed-33446382012-05-15 1-(4-Chloro­butano­yl)-3-(2-chloro­phen­yl)thio­urea Yusof, M. Sukeri M. Embong, Nur Farhana Yamin, Bohari M. Ngah, Nurziana Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(11)H(12)Cl(2)N(2)OS, contains two crystallographically independent mol­ecules with different conformations: the benzene ring and the thio­urea fragment form dihedral angles of 74.32 (11) and 89.39 (11)°. One amino group in each mol­ecule is involved in intra­molecular N—H⋯O and inter­molecular N—H⋯O hydrogen bonding: the latter links pairs of independent mol­ecules into dimers. In the crystal, weak N—H⋯S inter­actions link these dimers into chains propagating along the c axis. International Union of Crystallography 2012-04-25 /pmc/articles/PMC3344638/ /pubmed/22590400 http://dx.doi.org/10.1107/S160053681201759X Text en © Yusof et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Yusof, M. Sukeri M.
Embong, Nur Farhana
Yamin, Bohari M.
Ngah, Nurziana
1-(4-Chloro­butano­yl)-3-(2-chloro­phen­yl)thio­urea
title 1-(4-Chloro­butano­yl)-3-(2-chloro­phen­yl)thio­urea
title_full 1-(4-Chloro­butano­yl)-3-(2-chloro­phen­yl)thio­urea
title_fullStr 1-(4-Chloro­butano­yl)-3-(2-chloro­phen­yl)thio­urea
title_full_unstemmed 1-(4-Chloro­butano­yl)-3-(2-chloro­phen­yl)thio­urea
title_short 1-(4-Chloro­butano­yl)-3-(2-chloro­phen­yl)thio­urea
title_sort 1-(4-chloro­butano­yl)-3-(2-chloro­phen­yl)thio­urea
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344638/
https://www.ncbi.nlm.nih.gov/pubmed/22590400
http://dx.doi.org/10.1107/S160053681201759X
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AT ngahnurziana 14chlorobutanoyl32chlorophenylthiourea

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