N-(2-Nitro­phenyl­carbamothio­yl)acetamide

In the title compound, C(9)H(9)N(3)O(3)S, the benzene ring and the N-carbamothio­ylacetamide unit are oriented at a dihedral angle of 54.82 (4)°. The dihedral angle between the ring and its attached nitro group is 28.54 (12)°. An intra­molecular, bifurcated N—H⋯(O,O) hydrogen bond generates two S(6)...

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Detalles Bibliográficos
Autores principales: Shahwar, Durre, Tahir, M. Nawaz, Chohan, Muhammad Mansha, Khan, Muhammad Akmal, Ahmad, Nadeem
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344673/
https://www.ncbi.nlm.nih.gov/pubmed/22590435
http://dx.doi.org/10.1107/S1600536812016947
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author Shahwar, Durre
Tahir, M. Nawaz
Chohan, Muhammad Mansha
Khan, Muhammad Akmal
Ahmad, Nadeem
author_facet Shahwar, Durre
Tahir, M. Nawaz
Chohan, Muhammad Mansha
Khan, Muhammad Akmal
Ahmad, Nadeem
author_sort Shahwar, Durre
collection PubMed
description In the title compound, C(9)H(9)N(3)O(3)S, the benzene ring and the N-carbamothio­ylacetamide unit are oriented at a dihedral angle of 54.82 (4)°. The dihedral angle between the ring and its attached nitro group is 28.54 (12)°. An intra­molecular, bifurcated N—H⋯(O,O) hydrogen bond generates two S(6) rings. In the crystal, inversion dimers linked by pairs of N—H⋯S hydrogen bonds generate R (2) (2)(8) loops. Weak C—H⋯O inter­actions link the dimers.
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spelling pubmed-33446732012-05-15 N-(2-Nitro­phenyl­carbamothio­yl)acetamide Shahwar, Durre Tahir, M. Nawaz Chohan, Muhammad Mansha Khan, Muhammad Akmal Ahmad, Nadeem Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(9)H(9)N(3)O(3)S, the benzene ring and the N-carbamothio­ylacetamide unit are oriented at a dihedral angle of 54.82 (4)°. The dihedral angle between the ring and its attached nitro group is 28.54 (12)°. An intra­molecular, bifurcated N—H⋯(O,O) hydrogen bond generates two S(6) rings. In the crystal, inversion dimers linked by pairs of N—H⋯S hydrogen bonds generate R (2) (2)(8) loops. Weak C—H⋯O inter­actions link the dimers. International Union of Crystallography 2012-04-28 /pmc/articles/PMC3344673/ /pubmed/22590435 http://dx.doi.org/10.1107/S1600536812016947 Text en © Shahwar et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Shahwar, Durre
Tahir, M. Nawaz
Chohan, Muhammad Mansha
Khan, Muhammad Akmal
Ahmad, Nadeem
N-(2-Nitro­phenyl­carbamothio­yl)acetamide
title N-(2-Nitro­phenyl­carbamothio­yl)acetamide
title_full N-(2-Nitro­phenyl­carbamothio­yl)acetamide
title_fullStr N-(2-Nitro­phenyl­carbamothio­yl)acetamide
title_full_unstemmed N-(2-Nitro­phenyl­carbamothio­yl)acetamide
title_short N-(2-Nitro­phenyl­carbamothio­yl)acetamide
title_sort n-(2-nitro­phenyl­carbamothio­yl)acetamide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344673/
https://www.ncbi.nlm.nih.gov/pubmed/22590435
http://dx.doi.org/10.1107/S1600536812016947
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