Cargando…

[(3aS,5aR,8aR,8bS)-2,2,7,7-Tetramethyltetrahydro-3aH-bis[1,3]dioxolo[4,5-b:4′,5′-d]pyran-3a-yl]methyl (R)-N-(1-phenylethyl)sulfamate

In the title compound, C(20)H(29)NO(8)S, the two five-membered rings adopt envelope conformations (with an O atom at the flap in each case), while the six-membered pyran ring displays a twist-boat conformation. In the crystal, molecules are linked by N—H⋯O hydrogen bonds into a supramolecular chai...

Descripción completa

Detalles Bibliográficos
Autores principales:	Xie, Meng, Shen, Si-Si, Chen, Bao-Feng, Sha, Yu
Formato:	Online Artículo Texto
Lenguaje:	English
Publicado:	International Union of Crystallography 2012
Materias:	Organic Papers
Acceso en línea:	https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3344676/ https://www.ncbi.nlm.nih.gov/pubmed/22590438 http://dx.doi.org/10.1107/S1600536812016704

Ejemplares similares

Crystal structure, Hirshfeld surface analysis and corrosion inhibition study of 3,6-bis(pyridin-2-yl)-4-{[(3aS,5S,5aR,8aR,8bS)-2,2,7,7-tetramethyltetrahydro-5H-bis[1,3]dioxolo[4,5-b:4′,5′-d]pyran-5-yl)methoxy]methyl}pyridazine monohydrate
por: Filali, Mouad, et al.
Publicado: (2019)

Ethyl 1′-methyl-2-oxo-4′-[(3aR,5R,5aS,8aS,8bR)-2,2,7,7-tetramethyltetrahydro-3aH-bis[1,3]dioxolo[4,5-b:4′,5′-d]pyran-5-yl]-2H-spiro[acenaphthylene-1,2′-pyrrolidine]-3′-carboxylate
por: Jagadeesan, G., et al.
Publicado: (2013)

(3aR,8aR)-2,2,6,6-Tetramethyl-4,4,8,8-tetraphenyltetrahydro-1,3-dioxolo[4,5-e][1,3,2]dioxasilepine
por: Hijji, Yousef M., et al.
Publicado: (2008)

Ethyl (1R,1′S,2′S,7a’R)-2-oxo-1′-[(3aR,5R,5aS,8aS,8bR)-2,2,7,7-tetramethyltetrahydro-3aH-bis[1,3]dioxolo[4,5-b:4′,5′-d]pyran-5-yl]-1′,2′,5′,6′,7′,7a’-hexahydro-2H-spiro[acenaphthylene-1,3′-pyrrolizine]-2′-carboxylate
por: Jagadeesan, G., et al.
Publicado: (2012)

Ethyl (3S)-3-[(3aR,5R,6S,6aR)-6-hydroxy-2,2-dimethyltetrahydrofuro[4,5-d][1,3]dioxol-5-yl]-3-{(3S)-3-[(3aR,5R,6S,6aR)-6-hydroxy-2,2-dimethyltetrahydrofuro[4,5-d][1,3]dioxol-5-yl]-5-oxoisoxazolidin-2-yl}propanoate chloroform monosolvate
por: Amaro Hernández, Aldo Guillermo, et al.
Publicado: (2020)

{(3aR,5S,6R,6aR)-5-[(R)-1,2-Dihydroxyethyl]-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-6-yl}methyl methanesulfonate
por: Rjabovs, Vitālijs, et al.
Publicado: (2014)

(2S,3R,4S,4aR)-2,3,4,7-Tetrahydroxy-3,4,4a,5-tetrahydro[1,3]dioxolo[4,5-j]phenanthridin-6(2H)-one hemihydrate
por: Jucov, Evgheni, et al.
Publicado: (2012)

[(2S,3aR,6aR)-5-Oxohexahydrofuro[3,2-b]furan-2-yl]methyl acetate
por: González, María, et al.
Publicado: (2013)

(4aS,5R,7R,8S,8aR)-8-(1,3-Dioxolan-2-yl)-7,8-dimethyl-5-(1-methylethenyl)perhydronaphthalen-2-one
por: Siegler, Maxime A., et al.
Publicado: (2007)

6a-Nitro-6-(2,2,7,7-tetramethyltetrahydro-3aH-bis[1,3]dioxolo[4,5-b:4′,5′-d]pyran-5-yl)-6a,6b,7,8,9,11a-hexahydro-6H-spiro[chromeno[3,4-a]pyrrolizine-11,11′-indeno[1,2-b]quinoxaline]
por: Anuradha, T., et al.
Publicado: (2013)

Crystal structure of (1R,3aR,7aR)-1-{(S)-1-[(2R,5S)-5-(3-hydroxypentan-3-yl)tetrahydrofuran-2-yl]ethyl}-7a-methyl-2,3,3a,4,5,6,7,7a-octahydro-1H-inden-4-one
por: Martínez, Andrea, et al.
Publicado: (2017)

(3R*,5′S*)-6,7-Dimethoxy-3-(4′-methoxy-6′-methyl-5′,6′,7′,8′-tetrahydro-1,3-dioxolo[4,5-g]isoquinolin-5′-yl)isobenzofuran-1(3H)-one (racemic α-noscapine)
por: von Langermann, Jan, et al.
Publicado: (2010)

Tetrakis(2,3,5,5-tetramethylhexen-2-yl)silane
por: Meyer-Wegner, Frank, et al.
Publicado: (2014)

(±)-(4aR,5R,8S,8aR)-8-(tert-Butyldimethylsilyloxy)-2,5,8a-trimethyl-4a,5,8,8a-tetrahydronaphthalene-1,4-dione
por: Delling, Felix N., et al.
Publicado: (2013)

4,4,5,5-Tetramethyl-2-[1,3,6,8-tetrabromo-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyren-2-yl]-1,3,2-dioxaborolane
por: Chen, Ying, et al.
Publicado: (2012)

4,4′-Dichloro-3,3′,5,5′-tetramethyl-2,2′-[(3aR,7aR/3aS,7aS)-2,3,3a,4,5,6,7,7a-octahydro-1H-1,3-benzimidazole-1,3-diyl)bis(methylene)]diphenol
por: Rivera, Augusto, et al.
Publicado: (2011)

2-({3-[(2R,4S,5R)-4-Hydroxy-5-hydroxymethyl-2,3,4,5-tetrahydrofuran-2-yl]-5-methyl-2,6-dioxo-1,2,3,6-tetrahydropyrimidin-1-yl}methyl)isoindoline-1,3-dione
por: Bartholomä, Mark Daniel, et al.
Publicado: (2009)

1-[(2R,4aR,8R,8aR)-8-Hydroxy-4a,8-dimethylperhydronaphthalen-2-yl]ethan-1-one
por: Tebbaa, Mohamed, et al.
Publicado: (2011)

[(2R,3S,5R)-3-Acetoxy-5-(5-formyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-1-yl)-2,3,4,5-tetrahydrofuran-2-yl]methyl acetate
por: Jia, Xue-Fei, et al.
Publicado: (2011)

rac-(3aR,6aR)-(E)-Methyl 2-(3a-methylperhydrofuro[3,2-b]furan-2-ylidene)acetate
por: Bellovičová, Lenka, et al.
Publicado: (2010)

Pentafluorophenyl (3R,4R,5S)-5-{[(3R,4R,5S)-5-azidomethyl-3,4-dimethoxy-2,3,4,5-tetrahydrofuran-3-carboxamido]methyl}-3,4-dimethoxy-2,3,4,5-tetrahydrofuran-3-carboxylate
por: Simone, Michela I., et al.
Publicado: (2010)

(3R,4S,5S)-4-Hydroxy-3-methyl-5-[(2S,3R)-3-methylpent-4-en-2-yl]tetrahydrofuran-2-one
por: Becker, Annika, et al.
Publicado: (2008)

2,2,7,7-Tetramethyl-1,2,3,4,5,6,7,8-octahydroacridine-1,8-dione
por: Öztürk Yildirim, Sema, et al.
Publicado: (2012)

2,2,7,7-Tetramethyl-1,2,3,6,7,8-hexahydrocinnolino[5,4,3-cde]cinnoline
por: Peng, Ju-Hua, et al.
Publicado: (2009)

Steviamine, a new class of indolizidine alkaloid [(1R,2S,3R,5R,8aR)-3-hydroxymethyl-5-methyloctahydroindolizine-1,2-diol hydrobromide]
por: Thompson, Amber L., et al.
Publicado: (2009)

(1R,1′R,3S,3′S)-5,5′,10,10′-Tetramethoxy-1,1′,3,3′-tetramethyl-3,3′,4,4′-tetrahydro-1H,1′H-8,8′-bi[benzo[g]isochromene]
por: Sejberg, Jimmy J. P., et al.
Publicado: (2008)

(2S,3′S,3a’R,5′R,7a’R)-5′-[(E)-5-(Furan-3-yl)-2-methylpent-1-en-1-yl]-3-hydroxy-3′,4,7′-trimethyl-1′,2′,3′,3a’,5′,7a’-hexahydro-5H-spiro[furan-2,4′-inden]-5-one
por: Majer, Thomas, et al.
Publicado: (2020)

(6aR,10aR)-6,6,9-Trimethyl-3-pentyl-6a,7,8,10a-tetrahydro-6H-benzo[c]chromen-1-yl 4-methylbenzenesulfonate
por: Gul, Waseem, et al.
Publicado: (2008)

2,3-Bis(methylsulfanyl)-1,4,5,8-tetrathiafulvalene
por: Zheng, Ning-Juan, et al.
Publicado: (2010)

(1S*,4aR*,5S*,6S*,8aR*)-3-Benzyl-1-methyl-5,6-diphenyl-3,4,4a,5,6,8a-hexahydro-1H-2,3-benzoxazin-4-one
por: Wang, Yan, et al.
Publicado: (2009)

(4aR,8aR)-2,3-Diphenyl-4a,5,6,7,8,8a-hexahydroquinoxaline
por: Wang, Guo-Xi, et al.
Publicado: (2008)

Crystal structure of 4-methyl-N-{(E)-methyl[(3aR,8aS)-2-oxo-3,3a,8,8a-tetrahydro-2H-indeno[1,2-d][1,3]oxazol-3-yl]-λ(4)-sulfanylidene}benzenesulfonamide
por: Pereira, Patrícia A., et al.
Publicado: (2015)

(3aR*,5R*)-5-(4-Chlorophenyl)-1,2,3,3a-tetrahydrobenzo[e]pyrrolo[2,1-b][1,3]oxazepin-10(5H)-one
por: Jin, Yun-Zhou, et al.
Publicado: (2011)

rac-(4aR,8aR)-2,3-Diphenyl-4a,5,6,7,8,8a-hexahydroquinoxaline
por: Chen, Fang, et al.
Publicado: (2008)

3,3′,5,5′-Tetranitrobiphenyl
por: Hammond, N., et al.
Publicado: (2009)

Crystal structure of 2,3,5,6-tetrakis[(methylsulfanyl)methyl]pyrazine
por: Assoumatine, Tokouré, et al.
Publicado: (2014)

3-(4-Chlorophenyl)-1-[(2R,4aR,8aR)-4a,8-dimethyl-1,2,3,4,4a,5,6,8a-octahydronaphthalen-2-yl]prop-2-en-1-one
por: Tebbaa, Mohamed, et al.
Publicado: (2011)

(R)-N-Methyl-4-[2-(methylsulfanyl)pyrimidin-4-yl]-1-(tetrahydrofuran-3-yl)-1H-pyrazol-5-amine
por: Liu, Zhengyu, et al.
Publicado: (2009)

Crystal structure of (±)-(3aR,5R,8bR)-5-hydroperoxy-2-phenyl-6-tosyl-4,5,6,8b-tetrahydropyrrolo[3,4-e]indole-1,3(2H,3aH)-dione
por: Noland, Wayland E., et al.
Publicado: (2014)

7,11-Bis(4-methylphenyl)-2,4,8,10-tetraazaspiro[5.5]undecane-1,3,5,9-tetraone
por: Astaraki, Ali Mohammad, et al.
Publicado: (2008)

Cannot write session to /tmp/vufind_sessions/sess_38uo2009ecqg5ndktpc4nap6of