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Bismuth nitrate-induced microwave-assisted expeditious synthesis of vanillin from curcumin
BACKGROUND: Curcumin and vanillin are the two useful compounds in food and medicine. Bismuth nitrate pentahydrate is an economical and ecofriendly reagent. METHOD: Bismuth nitrate pentahydrate impregnated montmorillonite KSF clay and curcumin were subjected to microwave irradiation. RESULTS: Microwa...
Autores principales: | , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Springer
2012
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3364841/ https://www.ncbi.nlm.nih.gov/pubmed/22519970 http://dx.doi.org/10.1186/2191-2858-2-15 |
Sumario: | BACKGROUND: Curcumin and vanillin are the two useful compounds in food and medicine. Bismuth nitrate pentahydrate is an economical and ecofriendly reagent. METHOD: Bismuth nitrate pentahydrate impregnated montmorillonite KSF clay and curcumin were subjected to microwave irradiation. RESULTS: Microwave-induced bismuth nitrate-promoted synthesis of vanillin from curcumin has been accomplished in good yield under solvent-free condition. Twenty-five different reaction conditions have been studied to optimize the process. CONCLUSION: The present procedure for the synthesis of vanillin may find useful application in the area of industrial process development. |
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