Methyl 2-[(3,5-di-tert-butyl-4-hy­droxy­benz­yl)sulfan­yl]pyridine-3-carboxyl­ate n-hexane hemisolvate

The title solvated ester, C(22)H(29)NO(3)S·0.5C(6)H(14), crystallizes with two independent mol­ecules along with a hexane mol­ecule in the asymmetric unit. The two aromatic rings are separated by an –CH(2)–S– linkage; the rings are aligned at 83.27 (4)° in one mol­ecule and 47.66 (7)° in the other....

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Detalles Bibliográficos
Autores principales: Ariffin, Azhar, Nordin, Nordiana, Yehye, Wagee A., Ng, Seik Weng
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3379213/
https://www.ncbi.nlm.nih.gov/pubmed/22719411
http://dx.doi.org/10.1107/S1600536812018739
Descripción
Sumario:The title solvated ester, C(22)H(29)NO(3)S·0.5C(6)H(14), crystallizes with two independent mol­ecules along with a hexane mol­ecule in the asymmetric unit. The two aromatic rings are separated by an –CH(2)–S– linkage; the rings are aligned at 83.27 (4)° in one mol­ecule and 47.66 (7)° in the other. The hy­droxy group of one mol­ecule forms an O—H⋯O hydrogen bond to the other mol­ecule.

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