Cargando…

N-[2-(2-Hy­droxy­eth­oxy)pheneth­yl]phthalimide

The title compound, C(18)H(17)NO(4), was obtained accidentally through acid-catalysed aromatization of a phthalimide-substituted 2-(1-hy­droxy­eth­yl)cyclo­hex-2-enone. It exhibits an intra­molecular O—H⋯O(c) (c = carbonyl) hydrogen bond and forms a three-dimensional network structure via π–π stacki...

Descripción completa

Detalles Bibliográficos
Autores principales: Yang, Er-Qun, Zhang, Jun-Tao, Cao, Xiao-Ping, Gu, Jin-Zhong
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3379239/
https://www.ncbi.nlm.nih.gov/pubmed/22719437
http://dx.doi.org/10.1107/S1600536812018429
_version_ 1782236154242793472
author Yang, Er-Qun
Zhang, Jun-Tao
Cao, Xiao-Ping
Gu, Jin-Zhong
author_facet Yang, Er-Qun
Zhang, Jun-Tao
Cao, Xiao-Ping
Gu, Jin-Zhong
author_sort Yang, Er-Qun
collection PubMed
description The title compound, C(18)H(17)NO(4), was obtained accidentally through acid-catalysed aromatization of a phthalimide-substituted 2-(1-hy­droxy­eth­yl)cyclo­hex-2-enone. It exhibits an intra­molecular O—H⋯O(c) (c = carbonyl) hydrogen bond and forms a three-dimensional network structure via π–π stacking inter­actions between adjacent benzene rings (phthalimide-to-phenyl­ene and phthalimide-to-phthalimide), with centroid–centroid distances of 3.8262 (6) and 3.6245 (5) Å.
format Online
Article
Text
id pubmed-3379239
institution National Center for Biotechnology Information
language English
publishDate 2012
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-33792392012-06-20 N-[2-(2-Hy­droxy­eth­oxy)pheneth­yl]phthalimide Yang, Er-Qun Zhang, Jun-Tao Cao, Xiao-Ping Gu, Jin-Zhong Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(18)H(17)NO(4), was obtained accidentally through acid-catalysed aromatization of a phthalimide-substituted 2-(1-hy­droxy­eth­yl)cyclo­hex-2-enone. It exhibits an intra­molecular O—H⋯O(c) (c = carbonyl) hydrogen bond and forms a three-dimensional network structure via π–π stacking inter­actions between adjacent benzene rings (phthalimide-to-phenyl­ene and phthalimide-to-phthalimide), with centroid–centroid distances of 3.8262 (6) and 3.6245 (5) Å. International Union of Crystallography 2012-05-05 /pmc/articles/PMC3379239/ /pubmed/22719437 http://dx.doi.org/10.1107/S1600536812018429 Text en © Yang et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Yang, Er-Qun
Zhang, Jun-Tao
Cao, Xiao-Ping
Gu, Jin-Zhong
N-[2-(2-Hy­droxy­eth­oxy)pheneth­yl]phthalimide
title N-[2-(2-Hy­droxy­eth­oxy)pheneth­yl]phthalimide
title_full N-[2-(2-Hy­droxy­eth­oxy)pheneth­yl]phthalimide
title_fullStr N-[2-(2-Hy­droxy­eth­oxy)pheneth­yl]phthalimide
title_full_unstemmed N-[2-(2-Hy­droxy­eth­oxy)pheneth­yl]phthalimide
title_short N-[2-(2-Hy­droxy­eth­oxy)pheneth­yl]phthalimide
title_sort n-[2-(2-hy­droxy­eth­oxy)pheneth­yl]phthalimide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3379239/
https://www.ncbi.nlm.nih.gov/pubmed/22719437
http://dx.doi.org/10.1107/S1600536812018429
work_keys_str_mv AT yangerqun n22hydroxyethoxyphenethylphthalimide
AT zhangjuntao n22hydroxyethoxyphenethylphthalimide
AT caoxiaoping n22hydroxyethoxyphenethylphthalimide
AT gujinzhong n22hydroxyethoxyphenethylphthalimide