(E)-N′-Hy­droxy-1,3-diphenyl-4,5-di­hydro-1H-pyrazole-5-carboximidamide

In the mol­ecule of the title compound, C(16)H(16)N(4)O, the pyrazole ring makes dihedral angles of 8.52 (13) and 9.26 (12)° with the phenyl rings. The dihedral angle between the benzene rings is 1.86 (13)°. In the crystal, mol­ecules are linked into centrosymmetric dimers via pairs of O—H⋯N hydroge...

Descripción completa

Detalles Bibliográficos
Autores principales: Chandra, Srikantamurthy, N., Umesha, K. B., Jeyaseelan, S., Mahendra, M.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3379259/
https://www.ncbi.nlm.nih.gov/pubmed/22719457
http://dx.doi.org/10.1107/S1600536812019630
_version_ 1782236158891130880
author Chandra,
Srikantamurthy, N.
Umesha, K. B.
Jeyaseelan, S.
Mahendra, M.
author_facet Chandra,
Srikantamurthy, N.
Umesha, K. B.
Jeyaseelan, S.
Mahendra, M.
author_sort Chandra,
collection PubMed
description In the mol­ecule of the title compound, C(16)H(16)N(4)O, the pyrazole ring makes dihedral angles of 8.52 (13) and 9.26 (12)° with the phenyl rings. The dihedral angle between the benzene rings is 1.86 (13)°. In the crystal, mol­ecules are linked into centrosymmetric dimers via pairs of O—H⋯N hydrogen bonds. Weak N—H⋯N inter­actions connect the dimers into a chain along the [100] direction. The pyrazole ring adopts a highly flattened envelope conformation.
format Online
Article
Text
id pubmed-3379259
institution National Center for Biotechnology Information
language English
publishDate 2012
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-33792592012-06-20 (E)-N′-Hy­droxy-1,3-diphenyl-4,5-di­hydro-1H-pyrazole-5-carboximidamide Chandra, Srikantamurthy, N. Umesha, K. B. Jeyaseelan, S. Mahendra, M. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the mol­ecule of the title compound, C(16)H(16)N(4)O, the pyrazole ring makes dihedral angles of 8.52 (13) and 9.26 (12)° with the phenyl rings. The dihedral angle between the benzene rings is 1.86 (13)°. In the crystal, mol­ecules are linked into centrosymmetric dimers via pairs of O—H⋯N hydrogen bonds. Weak N—H⋯N inter­actions connect the dimers into a chain along the [100] direction. The pyrazole ring adopts a highly flattened envelope conformation. International Union of Crystallography 2012-05-05 /pmc/articles/PMC3379259/ /pubmed/22719457 http://dx.doi.org/10.1107/S1600536812019630 Text en © Chandra et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Chandra,
Srikantamurthy, N.
Umesha, K. B.
Jeyaseelan, S.
Mahendra, M.
(E)-N′-Hy­droxy-1,3-diphenyl-4,5-di­hydro-1H-pyrazole-5-carboximidamide
title (E)-N′-Hy­droxy-1,3-diphenyl-4,5-di­hydro-1H-pyrazole-5-carboximidamide
title_full (E)-N′-Hy­droxy-1,3-diphenyl-4,5-di­hydro-1H-pyrazole-5-carboximidamide
title_fullStr (E)-N′-Hy­droxy-1,3-diphenyl-4,5-di­hydro-1H-pyrazole-5-carboximidamide
title_full_unstemmed (E)-N′-Hy­droxy-1,3-diphenyl-4,5-di­hydro-1H-pyrazole-5-carboximidamide
title_short (E)-N′-Hy­droxy-1,3-diphenyl-4,5-di­hydro-1H-pyrazole-5-carboximidamide
title_sort (e)-n′-hy­droxy-1,3-diphenyl-4,5-di­hydro-1h-pyrazole-5-carboximidamide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3379259/
https://www.ncbi.nlm.nih.gov/pubmed/22719457
http://dx.doi.org/10.1107/S1600536812019630
work_keys_str_mv AT chandra enhydroxy13diphenyl45dihydro1hpyrazole5carboximidamide
AT srikantamurthyn enhydroxy13diphenyl45dihydro1hpyrazole5carboximidamide
AT umeshakb enhydroxy13diphenyl45dihydro1hpyrazole5carboximidamide
AT jeyaseelans enhydroxy13diphenyl45dihydro1hpyrazole5carboximidamide
AT mahendram enhydroxy13diphenyl45dihydro1hpyrazole5carboximidamide

Ejemplares similares