6-(4-Bromo­phen­yl)-3-methyl-7H-1,2,4-triazolo[3,4-b][1,3,4]thia­diazine

In the title compound, C(11)H(9)BrN(4)S, the 1,2,4-triazole ring is essentially planar (r.m.s. deviation = 0.020 Å) and makes a dihedral angle of 29.1 (5)° with the bromo­benzene ring. The 3,6-dihydro-1,3,4-thia­diazine ring adopts a twist-boat conformation. In the crystal, mol­ecules are linked by...

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Autores principales: Fun, Hoong-Kun, Quah, Ching Kheng, Abdel-Aziz, Hatem A., Attia, Mohamed I.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3379277/
https://www.ncbi.nlm.nih.gov/pubmed/22719475
http://dx.doi.org/10.1107/S1600536812019885
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author Fun, Hoong-Kun
Quah, Ching Kheng
Abdel-Aziz, Hatem A.
Attia, Mohamed I.
author_facet Fun, Hoong-Kun
Quah, Ching Kheng
Abdel-Aziz, Hatem A.
Attia, Mohamed I.
author_sort Fun, Hoong-Kun
collection PubMed
description In the title compound, C(11)H(9)BrN(4)S, the 1,2,4-triazole ring is essentially planar (r.m.s. deviation = 0.020 Å) and makes a dihedral angle of 29.1 (5)° with the bromo­benzene ring. The 3,6-dihydro-1,3,4-thia­diazine ring adopts a twist-boat conformation. In the crystal, mol­ecules are linked by C—H⋯N inter­actions into sheets lying parallel to the (010) plane. The same N atom accepts two such hydrogen bonds.
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spelling pubmed-33792772012-06-20 6-(4-Bromo­phen­yl)-3-methyl-7H-1,2,4-triazolo[3,4-b][1,3,4]thia­diazine Fun, Hoong-Kun Quah, Ching Kheng Abdel-Aziz, Hatem A. Attia, Mohamed I. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(11)H(9)BrN(4)S, the 1,2,4-triazole ring is essentially planar (r.m.s. deviation = 0.020 Å) and makes a dihedral angle of 29.1 (5)° with the bromo­benzene ring. The 3,6-dihydro-1,3,4-thia­diazine ring adopts a twist-boat conformation. In the crystal, mol­ecules are linked by C—H⋯N inter­actions into sheets lying parallel to the (010) plane. The same N atom accepts two such hydrogen bonds. International Union of Crystallography 2012-05-12 /pmc/articles/PMC3379277/ /pubmed/22719475 http://dx.doi.org/10.1107/S1600536812019885 Text en © Fun et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Fun, Hoong-Kun
Quah, Ching Kheng
Abdel-Aziz, Hatem A.
Attia, Mohamed I.
6-(4-Bromo­phen­yl)-3-methyl-7H-1,2,4-triazolo[3,4-b][1,3,4]thia­diazine
title 6-(4-Bromo­phen­yl)-3-methyl-7H-1,2,4-triazolo[3,4-b][1,3,4]thia­diazine
title_full 6-(4-Bromo­phen­yl)-3-methyl-7H-1,2,4-triazolo[3,4-b][1,3,4]thia­diazine
title_fullStr 6-(4-Bromo­phen­yl)-3-methyl-7H-1,2,4-triazolo[3,4-b][1,3,4]thia­diazine
title_full_unstemmed 6-(4-Bromo­phen­yl)-3-methyl-7H-1,2,4-triazolo[3,4-b][1,3,4]thia­diazine
title_short 6-(4-Bromo­phen­yl)-3-methyl-7H-1,2,4-triazolo[3,4-b][1,3,4]thia­diazine
title_sort 6-(4-bromo­phen­yl)-3-methyl-7h-1,2,4-triazolo[3,4-b][1,3,4]thia­diazine
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3379277/
https://www.ncbi.nlm.nih.gov/pubmed/22719475
http://dx.doi.org/10.1107/S1600536812019885
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