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1,4-Ditosyl-1,4-diazepane

In the title compound, C(19)H(24)N(2)O(4)S(2), the dihedral angle formed by the benzene rings is 82.88 (7)°, and the mol­ecular conformation is enforced by weak intra­molecular C—H⋯O contacts. Two C atoms of the 1,4-diazepane ring are disordered over two sets of sites with a refined occupancy ratio...

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Detalles Bibliográficos
Autores principales: Yang, Shuang-Hua, Zhai, Zhi-Wei
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3379307/
https://www.ncbi.nlm.nih.gov/pubmed/22719505
http://dx.doi.org/10.1107/S1600536812020958
Descripción
Sumario:In the title compound, C(19)H(24)N(2)O(4)S(2), the dihedral angle formed by the benzene rings is 82.88 (7)°, and the mol­ecular conformation is enforced by weak intra­molecular C—H⋯O contacts. Two C atoms of the 1,4-diazepane ring are disordered over two sets of sites with a refined occupancy ratio of 0.534 (13):0.466 (13). In the crystal, mol­ecules are linked by weak inter­molecular C—H⋯O inter­actions into chains parallel to the a axis.