2,3-Dihydro­pyrrolo­[2,1-b]quinazoline-9(1H)-thione

In the crystal, mol­ecules of the title compound, C(11)H(10)N(2)S, are connected by C—H⋯N inter­actions around threefold axes. Furthermore, they form stacks along the c axis showing π–π inter­actions between pyrimidine rings [centroid–centroid distance = 3.721 (1) Å]. The central ring is essentially...

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Autores principales: Nasrullayev, Azizbek O., Elmuradov, Burkhon Zh., Turgunov, Kambarali K., Tashkhodjaev, Bakhodir, Shakhidoyatov, Khusnutdin M.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3379333/
https://www.ncbi.nlm.nih.gov/pubmed/22719531
http://dx.doi.org/10.1107/S1600536812021228
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author Nasrullayev, Azizbek O.
Elmuradov, Burkhon Zh.
Turgunov, Kambarali K.
Tashkhodjaev, Bakhodir
Shakhidoyatov, Khusnutdin M.
author_facet Nasrullayev, Azizbek O.
Elmuradov, Burkhon Zh.
Turgunov, Kambarali K.
Tashkhodjaev, Bakhodir
Shakhidoyatov, Khusnutdin M.
author_sort Nasrullayev, Azizbek O.
collection PubMed
description In the crystal, mol­ecules of the title compound, C(11)H(10)N(2)S, are connected by C—H⋯N inter­actions around threefold axes. Furthermore, they form stacks along the c axis showing π–π inter­actions between pyrimidine rings [centroid–centroid distance = 3.721 (1) Å]. The central ring is essentially planar with an r.m.s. deviation of 0.007 Å. The five-membered ring adopts an envelope conformation with the flap atom deviating by 0.241 (4) Å from the mean plane (r.m.s. deviation = 0.002 Å) through the other four ring atoms.
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spelling pubmed-33793332012-06-20 2,3-Dihydro­pyrrolo­[2,1-b]quinazoline-9(1H)-thione Nasrullayev, Azizbek O. Elmuradov, Burkhon Zh. Turgunov, Kambarali K. Tashkhodjaev, Bakhodir Shakhidoyatov, Khusnutdin M. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the crystal, mol­ecules of the title compound, C(11)H(10)N(2)S, are connected by C—H⋯N inter­actions around threefold axes. Furthermore, they form stacks along the c axis showing π–π inter­actions between pyrimidine rings [centroid–centroid distance = 3.721 (1) Å]. The central ring is essentially planar with an r.m.s. deviation of 0.007 Å. The five-membered ring adopts an envelope conformation with the flap atom deviating by 0.241 (4) Å from the mean plane (r.m.s. deviation = 0.002 Å) through the other four ring atoms. International Union of Crystallography 2012-05-16 /pmc/articles/PMC3379333/ /pubmed/22719531 http://dx.doi.org/10.1107/S1600536812021228 Text en © Nasrullayev et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Nasrullayev, Azizbek O.
Elmuradov, Burkhon Zh.
Turgunov, Kambarali K.
Tashkhodjaev, Bakhodir
Shakhidoyatov, Khusnutdin M.
2,3-Dihydro­pyrrolo­[2,1-b]quinazoline-9(1H)-thione
title 2,3-Dihydro­pyrrolo­[2,1-b]quinazoline-9(1H)-thione
title_full 2,3-Dihydro­pyrrolo­[2,1-b]quinazoline-9(1H)-thione
title_fullStr 2,3-Dihydro­pyrrolo­[2,1-b]quinazoline-9(1H)-thione
title_full_unstemmed 2,3-Dihydro­pyrrolo­[2,1-b]quinazoline-9(1H)-thione
title_short 2,3-Dihydro­pyrrolo­[2,1-b]quinazoline-9(1H)-thione
title_sort 2,3-dihydro­pyrrolo­[2,1-b]quinazoline-9(1h)-thione
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3379333/
https://www.ncbi.nlm.nih.gov/pubmed/22719531
http://dx.doi.org/10.1107/S1600536812021228
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