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N′(2),N′(5)-Bis[(E)-2-hydroxybenzylidene]-3,4-dimethylthiophene-2,5-dicarbohydrazide
In the title molecule, C(22)H(20)N(4)O(4)S, both C=N bonds are in an E conformation. The benzene rings form dihedral angles of 12.10 (13) and 25.17 (12)° with the thiophene ring. The dihedral angle between the two benzene rings is 17.59 (14)°. There are two intramolecular O—H⋯N hydrogen bonds. In...
Autores principales: | , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2012
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3379339/ https://www.ncbi.nlm.nih.gov/pubmed/22719537 http://dx.doi.org/10.1107/S1600536812020260 |
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author | Zhang, Shao-Lin Zhang, Ling Wen, Qin-Mei Geng, Rong-Xia Zhou, Cheng-He |
author_facet | Zhang, Shao-Lin Zhang, Ling Wen, Qin-Mei Geng, Rong-Xia Zhou, Cheng-He |
author_sort | Zhang, Shao-Lin |
collection | PubMed |
description | In the title molecule, C(22)H(20)N(4)O(4)S, both C=N bonds are in an E conformation. The benzene rings form dihedral angles of 12.10 (13) and 25.17 (12)° with the thiophene ring. The dihedral angle between the two benzene rings is 17.59 (14)°. There are two intramolecular O—H⋯N hydrogen bonds. In the crystal, N—H⋯O hydrogen bonds connect molecules into chains along [010]. |
format | Online Article Text |
id | pubmed-3379339 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2012 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-33793392012-06-20 N′(2),N′(5)-Bis[(E)-2-hydroxybenzylidene]-3,4-dimethylthiophene-2,5-dicarbohydrazide Zhang, Shao-Lin Zhang, Ling Wen, Qin-Mei Geng, Rong-Xia Zhou, Cheng-He Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title molecule, C(22)H(20)N(4)O(4)S, both C=N bonds are in an E conformation. The benzene rings form dihedral angles of 12.10 (13) and 25.17 (12)° with the thiophene ring. The dihedral angle between the two benzene rings is 17.59 (14)°. There are two intramolecular O—H⋯N hydrogen bonds. In the crystal, N—H⋯O hydrogen bonds connect molecules into chains along [010]. International Union of Crystallography 2012-05-16 /pmc/articles/PMC3379339/ /pubmed/22719537 http://dx.doi.org/10.1107/S1600536812020260 Text en © Zhang et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Zhang, Shao-Lin Zhang, Ling Wen, Qin-Mei Geng, Rong-Xia Zhou, Cheng-He N′(2),N′(5)-Bis[(E)-2-hydroxybenzylidene]-3,4-dimethylthiophene-2,5-dicarbohydrazide |
title |
N′(2),N′(5)-Bis[(E)-2-hydroxybenzylidene]-3,4-dimethylthiophene-2,5-dicarbohydrazide |
title_full |
N′(2),N′(5)-Bis[(E)-2-hydroxybenzylidene]-3,4-dimethylthiophene-2,5-dicarbohydrazide |
title_fullStr |
N′(2),N′(5)-Bis[(E)-2-hydroxybenzylidene]-3,4-dimethylthiophene-2,5-dicarbohydrazide |
title_full_unstemmed |
N′(2),N′(5)-Bis[(E)-2-hydroxybenzylidene]-3,4-dimethylthiophene-2,5-dicarbohydrazide |
title_short |
N′(2),N′(5)-Bis[(E)-2-hydroxybenzylidene]-3,4-dimethylthiophene-2,5-dicarbohydrazide |
title_sort | n′(2),n′(5)-bis[(e)-2-hydroxybenzylidene]-3,4-dimethylthiophene-2,5-dicarbohydrazide |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3379339/ https://www.ncbi.nlm.nih.gov/pubmed/22719537 http://dx.doi.org/10.1107/S1600536812020260 |
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