Methyl 2-(thio­phene-2-carboxamido)­benzoate

The title compound, C(13)H(11)NO(3)S, was synthesized from methyl anthranilate, triethyl­amine and 2-thio­phenoyl chloride in benzene. The mol­ecular conformation is stabilized by an intra­molecular N—H⋯O hydrogen bond. The dihedral angle between the rings is 2.74 (12)°. In the crystal, C—H⋯O inter­...

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Detalles Bibliográficos
Autores principales: Singh, Durga Prasad, Pratap, Seema, Butcher, Ray J., Gupta, Sushil K.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3379349/
https://www.ncbi.nlm.nih.gov/pubmed/22719547
http://dx.doi.org/10.1107/S160053681202082X
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author Singh, Durga Prasad
Pratap, Seema
Butcher, Ray J.
Gupta, Sushil K.
author_facet Singh, Durga Prasad
Pratap, Seema
Butcher, Ray J.
Gupta, Sushil K.
author_sort Singh, Durga Prasad
collection PubMed
description The title compound, C(13)H(11)NO(3)S, was synthesized from methyl anthranilate, triethyl­amine and 2-thio­phenoyl chloride in benzene. The mol­ecular conformation is stabilized by an intra­molecular N—H⋯O hydrogen bond. The dihedral angle between the rings is 2.74 (12)°. In the crystal, C—H⋯O inter­actions link neighbouring mol­ecules into a three-dimensional network.
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spelling pubmed-33793492012-06-20 Methyl 2-(thio­phene-2-carboxamido)­benzoate Singh, Durga Prasad Pratap, Seema Butcher, Ray J. Gupta, Sushil K. Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(13)H(11)NO(3)S, was synthesized from methyl anthranilate, triethyl­amine and 2-thio­phenoyl chloride in benzene. The mol­ecular conformation is stabilized by an intra­molecular N—H⋯O hydrogen bond. The dihedral angle between the rings is 2.74 (12)°. In the crystal, C—H⋯O inter­actions link neighbouring mol­ecules into a three-dimensional network. International Union of Crystallography 2012-05-16 /pmc/articles/PMC3379349/ /pubmed/22719547 http://dx.doi.org/10.1107/S160053681202082X Text en © Singh et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Singh, Durga Prasad
Pratap, Seema
Butcher, Ray J.
Gupta, Sushil K.
Methyl 2-(thio­phene-2-carboxamido)­benzoate
title Methyl 2-(thio­phene-2-carboxamido)­benzoate
title_full Methyl 2-(thio­phene-2-carboxamido)­benzoate
title_fullStr Methyl 2-(thio­phene-2-carboxamido)­benzoate
title_full_unstemmed Methyl 2-(thio­phene-2-carboxamido)­benzoate
title_short Methyl 2-(thio­phene-2-carboxamido)­benzoate
title_sort methyl 2-(thio­phene-2-carboxamido)­benzoate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3379349/
https://www.ncbi.nlm.nih.gov/pubmed/22719547
http://dx.doi.org/10.1107/S160053681202082X
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AT butcherrayj methyl2thiophene2carboxamidobenzoate
AT guptasushilk methyl2thiophene2carboxamidobenzoate

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