(E)-2-[2-(4-Chloro­benzyl­idene)hydrazin­yl]-4-[3-(morpholin-4-ium-4-yl)propyl­amino]­quinazolin-1-ium bis­(perchlorate)

In the title compound, C(22)H(27)ClN(6)O(2) (2+)·2ClO(4) (−), the mol­ecule adopts an E conformation about the C=N double bond. The quinazoline ring is approximately planar, with an r.m.s. deviation of 0.0432 Å, and forms a dihedral angle of 5.77 (4)° with the chloro­phenyl ring. The crystal packing...

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Detalles Bibliográficos
Autores principales: Jiang, Nan, Zuo, Jian, Zhu, Wenmin, Zhao, Xinjie, Zhai, Xin
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3379393/
https://www.ncbi.nlm.nih.gov/pubmed/22719591
http://dx.doi.org/10.1107/S1600536812021678
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author Jiang, Nan
Zuo, Jian
Zhu, Wenmin
Zhao, Xinjie
Zhai, Xin
author_facet Jiang, Nan
Zuo, Jian
Zhu, Wenmin
Zhao, Xinjie
Zhai, Xin
author_sort Jiang, Nan
collection PubMed
description In the title compound, C(22)H(27)ClN(6)O(2) (2+)·2ClO(4) (−), the mol­ecule adopts an E conformation about the C=N double bond. The quinazoline ring is approximately planar, with an r.m.s. deviation of 0.0432 Å, and forms a dihedral angle of 5.77 (4)° with the chloro­phenyl ring. The crystal packing features N—H⋯O hydrogen bonds.
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spelling pubmed-33793932012-06-20 (E)-2-[2-(4-Chloro­benzyl­idene)hydrazin­yl]-4-[3-(morpholin-4-ium-4-yl)propyl­amino]­quinazolin-1-ium bis­(perchlorate) Jiang, Nan Zuo, Jian Zhu, Wenmin Zhao, Xinjie Zhai, Xin Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(22)H(27)ClN(6)O(2) (2+)·2ClO(4) (−), the mol­ecule adopts an E conformation about the C=N double bond. The quinazoline ring is approximately planar, with an r.m.s. deviation of 0.0432 Å, and forms a dihedral angle of 5.77 (4)° with the chloro­phenyl ring. The crystal packing features N—H⋯O hydrogen bonds. International Union of Crystallography 2012-05-19 /pmc/articles/PMC3379393/ /pubmed/22719591 http://dx.doi.org/10.1107/S1600536812021678 Text en © Jiang et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Jiang, Nan
Zuo, Jian
Zhu, Wenmin
Zhao, Xinjie
Zhai, Xin
(E)-2-[2-(4-Chloro­benzyl­idene)hydrazin­yl]-4-[3-(morpholin-4-ium-4-yl)propyl­amino]­quinazolin-1-ium bis­(perchlorate)
title (E)-2-[2-(4-Chloro­benzyl­idene)hydrazin­yl]-4-[3-(morpholin-4-ium-4-yl)propyl­amino]­quinazolin-1-ium bis­(perchlorate)
title_full (E)-2-[2-(4-Chloro­benzyl­idene)hydrazin­yl]-4-[3-(morpholin-4-ium-4-yl)propyl­amino]­quinazolin-1-ium bis­(perchlorate)
title_fullStr (E)-2-[2-(4-Chloro­benzyl­idene)hydrazin­yl]-4-[3-(morpholin-4-ium-4-yl)propyl­amino]­quinazolin-1-ium bis­(perchlorate)
title_full_unstemmed (E)-2-[2-(4-Chloro­benzyl­idene)hydrazin­yl]-4-[3-(morpholin-4-ium-4-yl)propyl­amino]­quinazolin-1-ium bis­(perchlorate)
title_short (E)-2-[2-(4-Chloro­benzyl­idene)hydrazin­yl]-4-[3-(morpholin-4-ium-4-yl)propyl­amino]­quinazolin-1-ium bis­(perchlorate)
title_sort (e)-2-[2-(4-chloro­benzyl­idene)hydrazin­yl]-4-[3-(morpholin-4-ium-4-yl)propyl­amino]­quinazolin-1-ium bis­(perchlorate)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3379393/
https://www.ncbi.nlm.nih.gov/pubmed/22719591
http://dx.doi.org/10.1107/S1600536812021678
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