(1E,2E)-2-Methyl-3-phenyl­acryl­aldehyde thio­semicarbazone

In the crystal structure of the title compound, C(11)H(13)N(3)S, mol­ecules form centrosymmetric synthons with an R (2) (2)(8) graph-set motif, linked by pairs of N—H⋯S hydrogen bonds. The synthons are connected through further N—H⋯S hydrogen bonds, extending the packing to form a two-dimensional ne...

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Detalles Bibliográficos
Autores principales: Mendoza-Meroño, Rafael, García-Granda, Santiago
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3379410/
https://www.ncbi.nlm.nih.gov/pubmed/22719608
http://dx.doi.org/10.1107/S1600536812022386
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author Mendoza-Meroño, Rafael
García-Granda, Santiago
author_facet Mendoza-Meroño, Rafael
García-Granda, Santiago
author_sort Mendoza-Meroño, Rafael
collection PubMed
description In the crystal structure of the title compound, C(11)H(13)N(3)S, mol­ecules form centrosymmetric synthons with an R (2) (2)(8) graph-set motif, linked by pairs of N—H⋯S hydrogen bonds. The synthons are connected through further N—H⋯S hydrogen bonds, extending the packing to form a two-dimensional network lying parallel to (001). In addition, C—H⋯π inter­actions are observed.
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spelling pubmed-33794102012-06-20 (1E,2E)-2-Methyl-3-phenyl­acryl­aldehyde thio­semicarbazone Mendoza-Meroño, Rafael García-Granda, Santiago Acta Crystallogr Sect E Struct Rep Online Organic Papers In the crystal structure of the title compound, C(11)H(13)N(3)S, mol­ecules form centrosymmetric synthons with an R (2) (2)(8) graph-set motif, linked by pairs of N—H⋯S hydrogen bonds. The synthons are connected through further N—H⋯S hydrogen bonds, extending the packing to form a two-dimensional network lying parallel to (001). In addition, C—H⋯π inter­actions are observed. International Union of Crystallography 2012-05-23 /pmc/articles/PMC3379410/ /pubmed/22719608 http://dx.doi.org/10.1107/S1600536812022386 Text en © Mendoza-Meroño and García-Granda 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Mendoza-Meroño, Rafael
García-Granda, Santiago
(1E,2E)-2-Methyl-3-phenyl­acryl­aldehyde thio­semicarbazone
title (1E,2E)-2-Methyl-3-phenyl­acryl­aldehyde thio­semicarbazone
title_full (1E,2E)-2-Methyl-3-phenyl­acryl­aldehyde thio­semicarbazone
title_fullStr (1E,2E)-2-Methyl-3-phenyl­acryl­aldehyde thio­semicarbazone
title_full_unstemmed (1E,2E)-2-Methyl-3-phenyl­acryl­aldehyde thio­semicarbazone
title_short (1E,2E)-2-Methyl-3-phenyl­acryl­aldehyde thio­semicarbazone
title_sort (1e,2e)-2-methyl-3-phenyl­acryl­aldehyde thio­semicarbazone
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3379410/
https://www.ncbi.nlm.nih.gov/pubmed/22719608
http://dx.doi.org/10.1107/S1600536812022386
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