tert-Butyl 6-amino-5-cyano-2-(2-meth­oxy­eth­yl)nicotinate

The title compound, C(14)H(19)N(3)O(3), was synthesized by the reaction of 3-meth­oxy­propionitrile, tert-butyl bromo­acetate and eth­oxy­methyl­enemalononitrile. In the crystal, N—H⋯O hydrogen bonds link the mol­ecules into chains propagating along the b axis.

Detalles Bibliográficos
Autores principales: Chen, Yi-Ning, Zhao, Xing-Dong, Deng, Jie, Li, Qin-Geng
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3381644/
https://www.ncbi.nlm.nih.gov/pubmed/22737103
http://dx.doi.org/10.1107/S1600536812014328
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author Chen, Yi-Ning
Zhao, Xing-Dong
Deng, Jie
Li, Qin-Geng
author_facet Chen, Yi-Ning
Zhao, Xing-Dong
Deng, Jie
Li, Qin-Geng
author_sort Chen, Yi-Ning
collection PubMed
description The title compound, C(14)H(19)N(3)O(3), was synthesized by the reaction of 3-meth­oxy­propionitrile, tert-butyl bromo­acetate and eth­oxy­methyl­enemalononitrile. In the crystal, N—H⋯O hydrogen bonds link the mol­ecules into chains propagating along the b axis.
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spelling pubmed-33816442012-06-26 tert-Butyl 6-amino-5-cyano-2-(2-meth­oxy­eth­yl)nicotinate Chen, Yi-Ning Zhao, Xing-Dong Deng, Jie Li, Qin-Geng Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(14)H(19)N(3)O(3), was synthesized by the reaction of 3-meth­oxy­propionitrile, tert-butyl bromo­acetate and eth­oxy­methyl­enemalononitrile. In the crystal, N—H⋯O hydrogen bonds link the mol­ecules into chains propagating along the b axis. International Union of Crystallography 2012-04-13 /pmc/articles/PMC3381644/ /pubmed/22737103 http://dx.doi.org/10.1107/S1600536812014328 Text en © Chen et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Chen, Yi-Ning
Zhao, Xing-Dong
Deng, Jie
Li, Qin-Geng
tert-Butyl 6-amino-5-cyano-2-(2-meth­oxy­eth­yl)nicotinate
title tert-Butyl 6-amino-5-cyano-2-(2-meth­oxy­eth­yl)nicotinate
title_full tert-Butyl 6-amino-5-cyano-2-(2-meth­oxy­eth­yl)nicotinate
title_fullStr tert-Butyl 6-amino-5-cyano-2-(2-meth­oxy­eth­yl)nicotinate
title_full_unstemmed tert-Butyl 6-amino-5-cyano-2-(2-meth­oxy­eth­yl)nicotinate
title_short tert-Butyl 6-amino-5-cyano-2-(2-meth­oxy­eth­yl)nicotinate
title_sort tert-butyl 6-amino-5-cyano-2-(2-meth­oxy­eth­yl)nicotinate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3381644/
https://www.ncbi.nlm.nih.gov/pubmed/22737103
http://dx.doi.org/10.1107/S1600536812014328
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AT zhaoxingdong tertbutyl6amino5cyano22methoxyethylnicotinate
AT dengjie tertbutyl6amino5cyano22methoxyethylnicotinate
AT liqingeng tertbutyl6amino5cyano22methoxyethylnicotinate

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