6-Meth­oxy­meth­oxy-7-trifluoro­methyl-1,3-benzodioxole-5-carbaldehyde

The title compound, C(11)H(9)F(3)O(5), crystallizes with three mol­ecules in the asymmetric unit. One –CF(3) group is disordered by rotation, with the F atoms split over two sets of sites with occupancies which converged to 0.888 (6) and 0.112 (6). Weak π–π inter­actions are observed between adjacen...

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Autores principales: Wang, Yanfeng, Pan, Xinhui, Liu, Dexiu, Lou, Hong-Xiang
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3393257/
https://www.ncbi.nlm.nih.gov/pubmed/22807814
http://dx.doi.org/10.1107/S1600536812022490
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author Wang, Yanfeng
Pan, Xinhui
Liu, Dexiu
Lou, Hong-Xiang
author_facet Wang, Yanfeng
Pan, Xinhui
Liu, Dexiu
Lou, Hong-Xiang
author_sort Wang, Yanfeng
collection PubMed
description The title compound, C(11)H(9)F(3)O(5), crystallizes with three mol­ecules in the asymmetric unit. One –CF(3) group is disordered by rotation, with the F atoms split over two sets of sites with occupancies which converged to 0.888 (6) and 0.112 (6). Weak π–π inter­actions are observed between adjacent benzene rings [the shortest centroid–centroid distance is 3.8858 (4) Å], resulting in the formation of a supra­molecular chain along [100].
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spelling pubmed-33932572012-07-17 6-Meth­oxy­meth­oxy-7-trifluoro­methyl-1,3-benzodioxole-5-carbaldehyde Wang, Yanfeng Pan, Xinhui Liu, Dexiu Lou, Hong-Xiang Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(11)H(9)F(3)O(5), crystallizes with three mol­ecules in the asymmetric unit. One –CF(3) group is disordered by rotation, with the F atoms split over two sets of sites with occupancies which converged to 0.888 (6) and 0.112 (6). Weak π–π inter­actions are observed between adjacent benzene rings [the shortest centroid–centroid distance is 3.8858 (4) Å], resulting in the formation of a supra­molecular chain along [100]. International Union of Crystallography 2012-06-02 /pmc/articles/PMC3393257/ /pubmed/22807814 http://dx.doi.org/10.1107/S1600536812022490 Text en © Wang et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wang, Yanfeng
Pan, Xinhui
Liu, Dexiu
Lou, Hong-Xiang
6-Meth­oxy­meth­oxy-7-trifluoro­methyl-1,3-benzodioxole-5-carbaldehyde
title 6-Meth­oxy­meth­oxy-7-trifluoro­methyl-1,3-benzodioxole-5-carbaldehyde
title_full 6-Meth­oxy­meth­oxy-7-trifluoro­methyl-1,3-benzodioxole-5-carbaldehyde
title_fullStr 6-Meth­oxy­meth­oxy-7-trifluoro­methyl-1,3-benzodioxole-5-carbaldehyde
title_full_unstemmed 6-Meth­oxy­meth­oxy-7-trifluoro­methyl-1,3-benzodioxole-5-carbaldehyde
title_short 6-Meth­oxy­meth­oxy-7-trifluoro­methyl-1,3-benzodioxole-5-carbaldehyde
title_sort 6-meth­oxy­meth­oxy-7-trifluoro­methyl-1,3-benzodioxole-5-carbaldehyde
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3393257/
https://www.ncbi.nlm.nih.gov/pubmed/22807814
http://dx.doi.org/10.1107/S1600536812022490
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AT liudexiu 6methoxymethoxy7trifluoromethyl13benzodioxole5carbaldehyde
AT louhongxiang 6methoxymethoxy7trifluoromethyl13benzodioxole5carbaldehyde

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