(E)-N′-(5-Bromo-2-hy­droxy-3-meth­oxy­benzyl­idene)-2-hy­droxy­benzohydrazide monohydrate

The organic molecule of the title hydrate, C(15)H(13)BrN(2)O(4)·H(2)O, is roughly planar, with a mean deviation of 0.0939 (2) Å. The dihedral angle between the two aromatic rings is 8.2 (3)°. Intra­molecular O—H⋯N and O—H⋯O hydrogen bonds are observed. In the crystal, N—H⋯O(water) and O(water)—H⋯O h...

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Detalles Bibliográficos
Autores principales: Zhao, Shunsheng, Li, Lanlan, Liu, Xiangrong, Feng, Weixu, Lü, Xingqiang
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2012
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3393308/
https://www.ncbi.nlm.nih.gov/pubmed/22807865
http://dx.doi.org/10.1107/S1600536812024816
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author Zhao, Shunsheng
Li, Lanlan
Liu, Xiangrong
Feng, Weixu
Lü, Xingqiang
author_facet Zhao, Shunsheng
Li, Lanlan
Liu, Xiangrong
Feng, Weixu
Lü, Xingqiang
author_sort Zhao, Shunsheng
collection PubMed
description The organic molecule of the title hydrate, C(15)H(13)BrN(2)O(4)·H(2)O, is roughly planar, with a mean deviation of 0.0939 (2) Å. The dihedral angle between the two aromatic rings is 8.2 (3)°. Intra­molecular O—H⋯N and O—H⋯O hydrogen bonds are observed. In the crystal, N—H⋯O(water) and O(water)—H⋯O hydrogen bonds lead to a three-dimensional network.
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spelling pubmed-33933082012-07-17 (E)-N′-(5-Bromo-2-hy­droxy-3-meth­oxy­benzyl­idene)-2-hy­droxy­benzohydrazide monohydrate Zhao, Shunsheng Li, Lanlan Liu, Xiangrong Feng, Weixu Lü, Xingqiang Acta Crystallogr Sect E Struct Rep Online Organic Papers The organic molecule of the title hydrate, C(15)H(13)BrN(2)O(4)·H(2)O, is roughly planar, with a mean deviation of 0.0939 (2) Å. The dihedral angle between the two aromatic rings is 8.2 (3)°. Intra­molecular O—H⋯N and O—H⋯O hydrogen bonds are observed. In the crystal, N—H⋯O(water) and O(water)—H⋯O hydrogen bonds lead to a three-dimensional network. International Union of Crystallography 2012-06-13 /pmc/articles/PMC3393308/ /pubmed/22807865 http://dx.doi.org/10.1107/S1600536812024816 Text en © Zhao et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zhao, Shunsheng
Li, Lanlan
Liu, Xiangrong
Feng, Weixu
Lü, Xingqiang
(E)-N′-(5-Bromo-2-hy­droxy-3-meth­oxy­benzyl­idene)-2-hy­droxy­benzohydrazide monohydrate
title (E)-N′-(5-Bromo-2-hy­droxy-3-meth­oxy­benzyl­idene)-2-hy­droxy­benzohydrazide monohydrate
title_full (E)-N′-(5-Bromo-2-hy­droxy-3-meth­oxy­benzyl­idene)-2-hy­droxy­benzohydrazide monohydrate
title_fullStr (E)-N′-(5-Bromo-2-hy­droxy-3-meth­oxy­benzyl­idene)-2-hy­droxy­benzohydrazide monohydrate
title_full_unstemmed (E)-N′-(5-Bromo-2-hy­droxy-3-meth­oxy­benzyl­idene)-2-hy­droxy­benzohydrazide monohydrate
title_short (E)-N′-(5-Bromo-2-hy­droxy-3-meth­oxy­benzyl­idene)-2-hy­droxy­benzohydrazide monohydrate
title_sort (e)-n′-(5-bromo-2-hy­droxy-3-meth­oxy­benzyl­idene)-2-hy­droxy­benzohydrazide monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3393308/
https://www.ncbi.nlm.nih.gov/pubmed/22807865
http://dx.doi.org/10.1107/S1600536812024816
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