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9-[(2-Methoxybenzyl)amino]-5-(3,4,5-trimethoxyphenyl)-5,5a,8a,9-tetrahydrofuro[3′,4′:6,7]naphtho[2,3-d][1,3]dioxol-6(8H)-one
In the title compound, C(30)H(31)NO(8), the tetrahydrofuran ring and the six-membered ring fused to it both display envelope conformations, both having the same C atom as the flap. The dihedral angles between the benzene ring of the benzo[d][1,3]dioxole ring system and the other two benzene rings...
| Autores principales: | , , , , |
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| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
International Union of Crystallography
2012
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| Materias: | |
| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3393313/ https://www.ncbi.nlm.nih.gov/pubmed/22807870 http://dx.doi.org/10.1107/S160053681202572X |
| _version_ | 1782237720518590464 |
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| author | Shi, Shaoyu Tian, Danli Luo, Gang Ai, Ting Chen, Hong |
| author_facet | Shi, Shaoyu Tian, Danli Luo, Gang Ai, Ting Chen, Hong |
| author_sort | Shi, Shaoyu |
| collection | PubMed |
| description | In the title compound, C(30)H(31)NO(8), the tetrahydrofuran ring and the six-membered ring fused to it both display envelope conformations, both having the same C atom as the flap. The dihedral angles between the benzene ring of the benzo[d][1,3]dioxole ring system and the other two benzene rings are 53.73 (3) and 83.30 (2)°. An intramolecular N—H⋯O hydrogen bond is present. In the crystal, weak intermolecular C—H⋯O hydrogen bonds link the molecules into chains parallel to the c axis. |
| format | Online Article Text |
| id | pubmed-3393313 |
| institution | National Center for Biotechnology Information |
| language | English |
| publishDate | 2012 |
| publisher | International Union of Crystallography |
| record_format | MEDLINE/PubMed |
| spelling | pubmed-33933132012-07-17 9-[(2-Methoxybenzyl)amino]-5-(3,4,5-trimethoxyphenyl)-5,5a,8a,9-tetrahydrofuro[3′,4′:6,7]naphtho[2,3-d][1,3]dioxol-6(8H)-one Shi, Shaoyu Tian, Danli Luo, Gang Ai, Ting Chen, Hong Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(30)H(31)NO(8), the tetrahydrofuran ring and the six-membered ring fused to it both display envelope conformations, both having the same C atom as the flap. The dihedral angles between the benzene ring of the benzo[d][1,3]dioxole ring system and the other two benzene rings are 53.73 (3) and 83.30 (2)°. An intramolecular N—H⋯O hydrogen bond is present. In the crystal, weak intermolecular C—H⋯O hydrogen bonds link the molecules into chains parallel to the c axis. International Union of Crystallography 2012-06-13 /pmc/articles/PMC3393313/ /pubmed/22807870 http://dx.doi.org/10.1107/S160053681202572X Text en © Shi et al. 2012 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
| spellingShingle | Organic Papers Shi, Shaoyu Tian, Danli Luo, Gang Ai, Ting Chen, Hong 9-[(2-Methoxybenzyl)amino]-5-(3,4,5-trimethoxyphenyl)-5,5a,8a,9-tetrahydrofuro[3′,4′:6,7]naphtho[2,3-d][1,3]dioxol-6(8H)-one |
| title | 9-[(2-Methoxybenzyl)amino]-5-(3,4,5-trimethoxyphenyl)-5,5a,8a,9-tetrahydrofuro[3′,4′:6,7]naphtho[2,3-d][1,3]dioxol-6(8H)-one |
| title_full | 9-[(2-Methoxybenzyl)amino]-5-(3,4,5-trimethoxyphenyl)-5,5a,8a,9-tetrahydrofuro[3′,4′:6,7]naphtho[2,3-d][1,3]dioxol-6(8H)-one |
| title_fullStr | 9-[(2-Methoxybenzyl)amino]-5-(3,4,5-trimethoxyphenyl)-5,5a,8a,9-tetrahydrofuro[3′,4′:6,7]naphtho[2,3-d][1,3]dioxol-6(8H)-one |
| title_full_unstemmed | 9-[(2-Methoxybenzyl)amino]-5-(3,4,5-trimethoxyphenyl)-5,5a,8a,9-tetrahydrofuro[3′,4′:6,7]naphtho[2,3-d][1,3]dioxol-6(8H)-one |
| title_short | 9-[(2-Methoxybenzyl)amino]-5-(3,4,5-trimethoxyphenyl)-5,5a,8a,9-tetrahydrofuro[3′,4′:6,7]naphtho[2,3-d][1,3]dioxol-6(8H)-one |
| title_sort | 9-[(2-methoxybenzyl)amino]-5-(3,4,5-trimethoxyphenyl)-5,5a,8a,9-tetrahydrofuro[3′,4′:6,7]naphtho[2,3-d][1,3]dioxol-6(8h)-one |
| topic | Organic Papers |
| url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3393313/ https://www.ncbi.nlm.nih.gov/pubmed/22807870 http://dx.doi.org/10.1107/S160053681202572X |
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